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3,6-双(氯甲基)杜烯

产品名称 3,6-双(氯甲基)杜烯

CAS号3022-16-0

分子式C12H16Cl2

分子量231.16

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  • Mass

    MS-IW-8183          
    1,4-bis(chloromethyl)-2,3,5,6-tetramethylbenzene
    C12H16Cl2           (Mass of molecular ion:    230)
    

       Source Temperature: 150 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          36.0       1.3
          39.0       1.3
          41.0       1.3
          51.0       1.5
          53.0       1.0
          64.0       2.1
          65.0       2.0
          71.0       2.4
          77.0       3.8
          78.0       1.7
          79.0       3.0
          91.0       2.8
          97.0       1.4
         105.0       2.5
         115.0       2.9
         117.0       1.7
         119.0       1.3
         127.0       1.1
         128.0       4.1
         129.0       5.2
         130.0       2.7
         131.0       1.7
         141.0       1.3
         143.0       1.7
         144.0       3.6
         145.0       6.1
         146.0       1.0
         147.0       1.3
         159.0      11.0
         160.0       8.5
         161.0       2.7
         162.0       1.0
         180.0       1.1
         181.0       2.2
         194.0       1.2
         195.0     100.0
         196.0      14.0
         197.0      33.2
         198.0       4.4
         230.0      25.4
         231.0       3.9
         232.0      16.4
         233.0       2.2
         234.0       2.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H16 Cl2 0.035 g : 0.5 ml CDCl3
    1,4-bis(chloromethyl)-2,3,5,6-tetramethylbenzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.685 B 2.343

         Hz     ppm     Int.
    

       1872.68   4.686    386
        936.52   2.344   1000
    

in CDCl3



KBr disc



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