图谱信息 供应商 相关产品
网站主页CAS数据库列表 2842-38-8更多图谱N-环己基单乙醇胺(2842-38-8)核磁图(13CNMR)

N-环己基单乙醇胺

产品名称 N-环己基单乙醇胺

CAS号2842-38-8

分子式C8H17NO

分子量143.23

展开


  • Mass

    MS-NW-8837          
    2-(cyclohexylamino)ethanol
    C8H17NO             (Mass of molecular ion:    143)
    

       Source Temperature: 270 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       1.8
          27.0       4.5
          28.0       7.9
          29.0       4.9
          30.0      93.1
          31.0       2.1
          39.0       4.6
          41.0      18.6
          42.0      10.8
          43.0       5.8
          44.0      11.3
          45.0       3.7
          53.0       3.0
          54.0       3.5
          55.0      30.8
          56.0      26.5
          57.0       1.8
          60.0       3.0
          62.0       1.2
          67.0       3.0
          68.0       3.4
          69.0       1.7
          70.0       5.9
          72.0       2.9
          74.0       1.0
          79.0       1.8
          80.0       1.5
          81.0       3.1
          82.0       8.3
          83.0      12.9
          84.0       1.6
          87.0       1.9
          96.0       1.5
          98.0       1.7
         100.0      53.4
         101.0       3.3
         110.0       1.0
         112.0     100.0
         113.0       8.3
         114.0       1.5
         142.0       1.7
         143.0       4.8
         144.0       2.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H17 N O 0.025 g : 0.5 ml CDCl3
    2-(cyclohexylamino)ethanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.646 B 2.86 C 2.781 D 2.431 E 1.902 F 1.734 G 1.619 J 1.25 K 1.20 L 1.08

         Hz     ppm     Int.
    

       1462.52   3.660    915
       1459.47   3.652    263
       1457.40   3.647    995
       1455.20   3.642    293
       1452.15   3.634   1000
       1144.29   2.864    245
       1121.95   2.808     41
       1121.46   2.807     41
       1116.70   2.795    964
       1113.77   2.787    280
       1111.45   2.782    990
       1109.50   2.777    313
       1106.32   2.769    925
        986.21   2.468     84
        982.42   2.459    173
        978.64   2.449    110
        975.71   2.442    186
        971.92   2.432    360
        968.14   2.423    207
        965.09   2.415    118
        961.30   2.406    195
        957.64   2.397    104
        768.55   1.924    268
        765.99   1.917    285
        762.21   1.908    181
        760.99   1.905    181
        755.98   1.892    291
        753.17   1.885    300
        706.54   1.768     72
        703.25   1.760    209
        699.58   1.751    300
        695.92   1.742    236
        689.94   1.727    264
        686.40   1.718    351
        684.20   1.712    247
        657.23   1.645    122
        655.40   1.640    147
        654.17   1.637    183
        652.59   1.633    133
        650.76   1.629    134
        649.41   1.625    117
        645.26   1.615    143
        642.58   1.608    183
        641.72   1.606    188
        640.26   1.603    126
        638.31   1.598    140
        634.77   1.589     57
        525.02   1.314     66
        521.73   1.306     95
        518.43   1.298     47
        512.94   1.284    179
        509.64   1.276    292
        506.71   1.268    160
        499.88   1.251    235
        497.07   1.244    398
        494.26   1.237    235
        489.87   1.226     59
        487.43   1.220    163
        484.25   1.212    257
        482.42   1.208    211
        480.83   1.204    218
        477.54   1.195    140
        471.56   1.180    132
        468.63   1.173    265
        465.33   1.165    152
        462.40   1.158     44
        459.96   1.151     82
        456.54   1.143    185
        453.25   1.135    100
        448.36   1.122    166
        444.70   1.113    173
        440.67   1.103     79
        435.91   1.091    307
        433.84   1.086    303
        425.42   1.065    251
        422.97   1.059    274
        413.70   1.036     89
        410.28   1.027    101
    

in CDCl3



KBr disc



nujol mull