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网站主页CAS数据库列表 2744-09-4更多图谱反-十氢异喹啉(2744-09-4)核磁图(13CNMR)

反-十氢异喹啉

产品名称 反-十氢异喹啉

CAS号2744-09-4

分子式C9H17N

分子量139.24

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  • Mass

    MS-KW-0414          
    trans-decahydroisoquinoline
    C9H17N              (Mass of molecular ion:    139)
    

       Source Temperature: 240 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       5.2
          28.0       3.7
          29.0       6.9
          30.0      46.2
          31.0       1.0
          39.0       7.6
          40.0       1.3
          41.0      16.9
          42.0      13.3
          43.0      32.0
          44.0     100.0
          45.0       3.6
          46.0       1.3
          51.0       1.2
          53.0       4.7
          54.0       6.0
          55.0      11.9
          56.0      24.8
          57.0      28.0
          58.0       3.0
          65.0       1.7
          66.0       1.0
          67.0      16.1
          68.0       5.9
          69.0       3.6
          70.0       6.3
          71.0       1.4
          77.0       2.1
          78.0       1.1
          79.0       6.2
          80.0       3.5
          81.0       6.1
          82.0      11.7
          83.0       3.4
          84.0       2.4
          85.0       1.1
          91.0       1.2
          93.0       4.3
          94.0       4.7
          95.0       3.5
          96.0      59.8
          97.0       6.2
          98.0       1.5
         107.0       1.2
         108.0       4.9
         109.0       4.5
         110.0       6.0
         111.0       2.7
         122.0       1.8
         124.0      10.6
         125.0       1.0
         136.0       1.0
         137.0       1.0
         138.0      40.8
         139.0      39.6
         140.0       4.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9H17N 0.05 ml : 0.5 ml CDCl3
    trans-decahydroisoquinoline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.041 B 2.867 C 2.615 D 2.232 E 1.71 F 1.58 G 1.51 J 1.27 L 1.03 M 0.91 assigned by C-H COSY

         Hz     ppm     Int.
    

       1223.64   3.061    295
       1222.05   3.057    353
       1220.46   3.053    291
       1211.55   3.031    321
       1209.84   3.027    377
       1208.26   3.023    312
       1152.96   2.884    409
       1150.64   2.879    388
       1142.22   2.858    435
       1138.68   2.849    412
       1058.35   2.648    451
       1055.55   2.641    470
       1046.15   2.617    821
       1043.34   2.610    807
       1033.94   2.587    424
       1031.13   2.580    404
        903.20   2.260    643
        892.83   2.234    702
        891.24   2.230    693
        880.86   2.204    627
        693.97   1.736    288
        690.92   1.729    415
        688.60   1.723    593
        686.28   1.717    579
        681.52   1.705    525
        679.45   1.700    555
        677.01   1.694    415
        633.92   1.586    343
        626.35   1.567    341
        610.60   1.528    687
        608.16   1.522    737
        597.91   1.496   1000
        595.34   1.490    926
        522.10   1.306    222
        518.56   1.298    353
        507.82   1.271    521
        479.25   1.199    165
        475.10   1.189    162
        468.14   1.171    224
        463.99   1.161    254
        455.69   1.140    302
        451.54   1.130    274
        443.00   1.109    230
        438.85   1.098    216
        433.96   1.086    234
        425.79   1.066    277
        422.61   1.058    350
        419.07   1.049    330
        415.65   1.040    295
        410.16   1.026    581
        400.64   1.003    617
        380.38   0.952    195
        377.20   0.944    207
        367.92   0.921    289
        364.51   0.912    318
        356.57   0.892    244
        353.03   0.884    243
        343.88   0.861    117
        340.46   0.852    123
    

in CDCl3