图谱信息 供应商 相关产品
网站主页CAS数据库列表 2657-00-3更多图谱2-重氮-1-萘酚-5-磺酸钠(2657-00-3)核磁图(1HNMR)

2-重氮-1-萘酚-5-磺酸钠

产品名称 2-重氮-1-萘酚-5-磺酸钠

CAS号2657-00-3

分子式C10H7N2NaO4S

分子量274.23

展开

400 MHz in DMSO-d6

90 MHz in D2O


  • 1H NMR 399.65 MHz
    C10 H5 N2 Na O4 S 0.040 g : 0.5 ml DMSO-d6
    sodium 6-diazo-5-oxo-5,6-dihydro-1-naphthalenesulfonate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.18 B 8.150 C 7.627 D 7.442 E 7.339 ASSIGNED BY H-H AND C-H COSY. J(C,E)=9.9HZ

         Hz     ppm     Int.
    

       3272.09   8.188    507
       3271.64   8.187    505
       3264.16   8.168    567
       3263.55   8.167    578
       3261.72   8.162    645
       3260.19   8.158    578
       3254.24   8.143    646
       3252.72   8.139    549
       3059.54   7.656     26
       3053.59   7.641    696
       3043.82   7.617    836
       2982.03   7.462    473
       2978.06   7.452     64
       2974.24   7.443    797
       2966.61   7.424    434
       2937.93   7.352   1000
       2933.04   7.340     50
       2931.82   7.336     47
       2928.01   7.327    858
    


  • 1H NMR 89.56 MHz
    C10 H5 N2 Na O4 S 0.042 g : 0.5 ml D2O
    sodium 6-diazo-5-oxo-5,6-dihydro-1-naphthalenesulfonate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.204 B 8.045 C 7.46 D 7.35 E 7.145 J(D,E)=9.9HZ

         Hz     ppm     Int.
    

        739.81   8.261    325
        738.50   8.246    411
        732.31   8.177    414
        731.19   8.165    493
        725.63   8.103    314
        724.88   8.094    315
        724.19   8.087    297
        717.56   8.013    414
        716.75   8.004    392
        674.75   7.535    408
        667.00   7.448    555
        665.44   7.431    389
        665.06   7.426    383
        659.13   7.360    286
        654.88   7.313    779
        642.94   7.179   1000
        633.06   7.069    404
    

in DMSO-d6



KBr disc