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网站主页CAS数据库列表 25542-62-5更多图谱6-溴己酸乙酯(25542-62-5)核磁图(1HNMR)

6-溴己酸乙酯

产品名称 6-溴己酸乙酯

CAS号25542-62-5

分子式C8H15BrO2

分子量223.11

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  • Mass

    MS-IW-5471          
    ethyl 6-bromohexanoate
    C8H15BrO2           (Mass of molecular ion:    222)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       1.1
          26.0       1.6
          27.0      10.5
          28.0       4.2
          29.0      18.2
          31.0       1.5
          39.0       6.3
          40.0       1.8
          41.0      21.6
          42.0       8.7
          43.0       7.9
          45.0       9.1
          48.0       1.4
          53.0       2.5
          54.0       2.1
          55.0      12.7
          56.0       1.0
          60.0      21.9
          61.0      13.1
          67.0       3.3
          68.0       4.6
          69.0      48.2
          70.0      14.9
          71.0       3.4
          73.0      12.5
          79.0       1.3
          80.0       3.9
          81.0       1.3
          82.0       3.9
          87.0       2.2
          88.0     100.0
          89.0       5.2
          96.0       3.4
          97.0      13.3
          98.0       1.0
         101.0      12.4
         107.0       2.1
         109.0       2.0
         115.0      16.3
         116.0       1.1
         143.0      11.1
         144.0       1.0
         149.0       1.8
         151.0       1.7
         177.0      16.3
         178.0       1.3
         179.0      16.2
         180.0       1.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H15 Br O2 0.05 ml : 0.5 ml CDCl3
    ethyl 6-bromohexanoate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.127 B 3.412 C 2.316 D 1.880 E 1.656 F 1.485 G 1.257

         Hz     ppm     Int.
    

       1660.28   4.155    193
       1653.20   4.137    524
       1646.00   4.119    527
       1638.92   4.101    202
       1370.61   3.430    340
       1363.89   3.413    625
       1357.06   3.396    353
        933.23   2.336    296
        925.90   2.317    485
        918.33   2.298    323
        765.87   1.917     78
        759.03   1.900    193
        756.59   1.894     59
        753.66   1.886     75
        751.71   1.881    205
        750.98   1.880    196
        746.83   1.869     46
        744.02   1.862    220
        737.30   1.845     93
        677.86   1.697     58
        670.53   1.678    167
        668.09   1.672     55
        662.60   1.658    202
        654.66   1.639    174
        647.58   1.621     87
        607.67   1.521     64
        606.81   1.519     74
        601.68   1.506     89
        599.37   1.500    152
        595.46   1.490     83
        592.04   1.482    207
        589.60   1.476     99
        586.79   1.469     69
        584.35   1.463     85
        583.37   1.460    101
        577.15   1.445     35
        576.17   1.442     41
        509.52   1.275    604
        502.32   1.257   1000
        495.12   1.239    600
    

in CDCl3



liquid film