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1-氨基四氢化萘

产品名称 1-氨基四氢化萘

CAS号2217-41-6

分子式C10H13N

分子量147.22

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  • Mass

    MS-NW-6428          
    5,6,7,8-tetrahydro-1-naphthylamine
    C10H13N             (Mass of molecular ion:    147)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          18.0       1.3
          27.0       1.9
          28.0       1.4
          30.0       1.0
          39.0       4.3
          41.0       1.8
          50.0       1.3
          51.0       3.6
          52.0       2.2
          53.0       1.8
          54.0       1.1
          58.5       2.8
          59.5       1.9
          63.0       2.5
          64.0       1.1
          64.5       1.4
          65.0       5.3
          65.5       3.3
          66.0       2.0
          71.5       3.6
          72.0       1.1
          72.5       1.6
          73.5       1.7
          77.0       4.8
          78.0       1.9
          79.0       1.4
          89.0       1.7
          90.0       1.2
          91.0       6.9
          92.0       2.7
          93.0       1.7
         102.0       1.2
         103.0       2.1
         104.0       2.1
         105.0       1.0
         106.0       9.2
         115.0       7.2
         116.0       2.2
         117.0       4.1
         118.0      10.8
         119.0      57.9
         120.0       5.9
         127.0       4.1
         128.0       4.5
         129.0       5.4
         130.0      12.0
         131.0      10.7
         132.0      12.3
         133.0       1.4
         143.0       4.2
         144.0       9.3
         145.0       7.2
         146.0      31.2
         147.0     100.0
         148.0      11.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H13 N 0.05 ml : 0.5 ml CDCl3
    5,6,7,8-tetrahydro-1-naphthylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.919 B 6.530 C 6.478 D 3.42 E 2.714 F 2.414 G *1 1.834 J *1 1.736

         Hz     ppm     Int.
    

       2773.07   6.939    374
       2765.38   6.920    758
       2757.69   6.901    442
       2613.04   6.539    550
       2609.25   6.529     93
       2605.47   6.520    521
       2600.34   6.507     55
       2599.73   6.506     54
       2596.56   6.498     72
       2596.19   6.497     72
       2593.38   6.490    573
       2592.77   6.488    591
       2588.26   6.477     58
       2585.57   6.470    512
       2584.96   6.469    527
       1366.09   3.419    345
       1095.95   2.743     52
       1090.82   2.730    505
       1084.59   2.714    891
       1078.61   2.699    535
        971.07   2.430    490
        964.84   2.415   1000
        958.25   2.398    574
        953.74   2.387     52
        745.97   1.867    216
        742.68   1.859    191
        739.62   1.851    411
        736.21   1.843    383
        734.50   1.838    567
        730.22   1.828    374
        728.27   1.823    651
        724.12   1.812    192
        723.63   1.811    190
        721.80   1.807    253
        717.04   1.795     94
        714.97   1.789     68
        713.13   1.785     56
        711.55   1.781     69
        710.57   1.778     64
        709.23   1.775     94
        708.62   1.774     91
        707.40   1.771     78
        705.44   1.766    120
        703.61   1.761    329
        701.66   1.756    284
        697.39   1.746    681
        695.43   1.741    520
        691.41   1.731    656
        689.21   1.725    470
        686.28   1.718    491
        683.11   1.710    200
        680.30   1.703    180
        679.81   1.702    174
    

in CDCl3



liquid film