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网站主页CAS数据库列表 21715-90-2更多图谱N-羟基-5-降冰片烯-2,3-二甲酰亚胺(21715-90-2)红外图谱(IR2)

N-羟基-5-降冰片烯-2,3-二甲酰亚胺

产品名称 N-羟基-5-降冰片烯-2,3-二甲酰亚胺

CAS号21715-90-2

分子式C9H9NO3

分子量179.17

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  • Mass

    MS-NW-6316          
    N-hydroxy-5-norbornene-2,3-dicarboximide
    C9H9NO3             (Mass of molecular ion:    179)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          17.0       1.1
          18.0       4.9
          26.0       3.2
          27.0       4.2
          37.0       1.0
          38.0       2.8
          39.0      12.2
          40.0       5.3
          41.0       2.4
          43.0       1.2
          44.0       2.6
          45.0       1.4
          46.0       1.1
          50.0       3.4
          51.0       7.1
          52.0       3.5
          53.0       3.0
          54.0       3.3
          55.0       4.7
          60.0       1.3
          62.0       2.1
          63.0       5.2
          64.0       2.1
          65.0      13.8
          65.5       5.4
          66.0     100.0
          66.5       1.3
          67.0       9.8
          70.0       1.1
          74.0       1.0
          75.0       1.1
          76.0       1.4
          77.0       9.0
          78.0       3.5
          79.0       3.8
          80.0       1.2
          85.0       1.9
          89.0       2.5
          90.0       1.7
          91.0      10.9
          92.0       3.8
          93.0       1.6
          97.0       1.5
          98.0       1.7
         102.0       1.2
         103.0       3.5
         104.0       3.5
         105.0       5.7
         106.0       5.0
         113.0       2.9
         114.0       9.0
         115.0       9.2
         116.0       2.8
         117.0       9.7
         118.0       2.7
         119.0       2.5
         130.0      10.1
         131.0       6.6
         132.0      82.6
         133.0      59.2
         134.0       6.5
         151.0       1.2
         164.0       3.1
         179.0       4.7
         181.0       1.4
         198.0       1.1
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C9 H9 N O3 0.041 g : 0.5 ml DMSO-d6
    N-hydroxy-5-norbornene-2,3-dicarboximide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 10.5 B 6.051 C *1 3.26 D *1 3.24 E *2 1.572 F *2 1.492

         Hz     ppm     Int.
    

       4208.22  10.530    636
       2420.20   6.056    499
       2418.67   6.052    818
       2417.14   6.049    567
       1309.20   3.276     25
       1304.63   3.265    267
       1301.73   3.258    570
       1300.35   3.254   1000
       1296.54   3.245    416
       1295.01   3.241    511
       1293.49   3.237    449
       1292.11   3.234    350
        635.38   1.590     98
        633.85   1.587    178
        632.48   1.583    124
        625.15   1.565    283
        623.93   1.562    205
        599.67   1.501    277
        590.97   1.479    175
    

in DMSO-d6



KBr disc



nujol mull



4880 A,200 M,powder