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网站主页CAS数据库列表 21545-54-0更多图谱N-环己基-N’-[2-(4-吗啉基)乙基]-硫脲(21545-54-0)质谱(MS)

N-环己基-N’-[2-(4-吗啉基)乙基]-硫脲

产品名称 N-环己基-N’-[2-(4-吗啉基)乙基]-硫脲

CAS号21545-54-0

分子式C13H25N3OS

分子量271.42


  • Mass

    MS-IW-0098          
    1-cyclohexyl-3-(2-morpholinoethyl)thiourea
    C13H25N3OS          (Mass of molecular ion:    271)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          27.0       2.0
          28.0       4.0
          29.0       3.1
          30.0       3.3
          34.0       1.0
          39.0       1.8
          41.0       6.7
          42.0       5.3
          43.0       2.6
          44.0       3.2
          53.0       1.1
          54.0       2.2
          55.0      14.5
          56.0      14.4
          57.0       2.9
          60.0       1.1
          67.0       2.6
          69.0       2.8
          70.0       5.7
          71.0       1.1
          72.0       1.8
          77.0       1.8
          81.0       1.6
          82.0       3.4
          83.0      10.0
          84.0       2.4
          85.0       1.3
          86.0       1.2
          98.0       9.2
          99.0       1.0
         100.0     100.0
         101.0       6.9
         103.0       3.3
         112.0       2.9
         113.0      74.6
         114.0       8.4
         141.0       9.4
         142.0       1.4
         155.0       1.2
         159.0      10.5
         160.0       1.0
         173.0       1.2
         184.0       2.6
         207.0       1.6
         237.0       3.4
         271.0       8.0
         272.0       1.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H25 N3 O S 0.046 g : 0.5 ml CDCl3
    1-cyclohexyl-3-(2-morpholinoethyl)thiourea
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.63 B 3.721 C 3.51 D 2.575 E 2.512 F 2.51 G 2.045 J 1.769 K 1.296 L 1.370 M 1.24 N 1.18

         Hz     ppm     Int.
    

       2650.02   6.631    136
       1491.70   3.733    754
       1487.18   3.722   1000
       1482.54   3.710    762
       1403.69   3.513    131
       1034.79   2.590    469
       1029.17   2.576    583
       1023.68   2.562    467
       1008.54   2.524    674
       1004.03   2.513    872
        999.51   2.501    645
        823.97   2.062    211
        819.21   2.050    168
        814.09   2.038    222
        718.14   1.797    158
        714.72   1.789    239
        710.94   1.779    190
        704.59   1.764    211
        701.05   1.755    289
        697.75   1.746    209
        673.58   1.686     91
        670.17   1.677    124
        666.38   1.668     95
        660.77   1.654    111
        657.10   1.645    141
        653.69   1.636     98
        543.95   1.362    265
        498.05   1.247    253
        495.48   1.240    251
        487.18   1.220    259
    

in CDCl3



KBr disc



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