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N-正丁基乙烯二胺

产品名称 N-正丁基乙烯二胺

CAS号19522-69-1

分子式C6H16N2

分子量116.2

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  • Mass

    MS-IW-4034          
    n-butylethylenediamine
    C6H16N2             (Mass of molecular ion:    116)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       5.8
          27.0       4.2
          28.0       6.5
          29.0      16.5
          30.0      65.2
          31.0       1.3
          39.0       2.4
          41.0      17.4
          42.0       7.6
          43.0       6.1
          44.0      72.4
          45.0       2.2
          55.0       3.2
          56.0       7.1
          57.0      16.3
          58.0       2.0
          70.0       2.7
          71.0       2.4
          72.0       2.3
          73.0       7.1
          83.0       1.6
          84.0       2.4
          85.0       2.2
          86.0     100.0
          87.0       6.7
          98.0       1.3
          99.0       2.1
         116.0       5.0
         117.0       1.2
         127.0       5.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H16 N2 0.05 ml : 0.5 ml CDCl3
    N-butylethylenediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.801 B 2.672 C 2.604 D 2.08 E 1.477 F 1.351 G 0.919

         Hz     ppm     Int.
    

       1125.73   2.817    106
       1120.00   2.803    191
       1114.14   2.788    140
       1072.88   2.685    187
       1066.89   2.670    208
       1061.16   2.656    105
       1048.22   2.623    160
       1041.02   2.605    232
       1033.69   2.587    168
        830.57   2.079    273
        606.57   1.518     60
        605.83   1.516     57
        599.61   1.501    144
        596.68   1.494     84
        592.41   1.483    169
        591.55   1.481    193
        590.94   1.479    194
        589.23   1.475     98
        584.11   1.462    178
        581.91   1.457    108
        577.15   1.445    103
        576.54   1.443    101
        557.50   1.395     59
        550.54   1.378    161
        542.60   1.358    201
        541.87   1.356    176
        534.79   1.339    210
        527.71   1.321    132
        520.75   1.304     50
        374.27   0.937    567
        366.94   0.919   1000
        359.74   0.901    469
    

in CDCl3



liquid film