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网站主页CAS数据库列表 19060-15-2更多图谱4-氨基丁醛二甲缩醛(19060-15-2)质谱(MS)

4-氨基丁醛二甲缩醛

产品名称 4-氨基丁醛二甲缩醛

CAS号19060-15-2

分子式C6H15NO2

分子量133.19

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  • Mass

    MS-IW-8662          
    4,4-dimethoxybutylamine
    C6H15NO2            (Mass of molecular ion:    133)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          14.0       1.4
          15.0       9.6
          18.0       3.4
          26.0       1.9
          27.0       7.7
          28.0      18.0
          29.0      22.3
          30.0      57.7
          31.0      53.4
          32.0      34.7
          33.0       2.1
          37.0       1.5
          38.0       2.5
          39.0      13.4
          40.0       7.0
          41.0      77.4
          42.0      38.3
          43.0     100.0
          44.0       6.0
          45.0       9.4
          47.0      15.6
          53.0       6.5
          54.0       3.1
          55.0      25.6
          56.0       3.8
          57.0       7.1
          58.0       3.2
          59.0       2.8
          67.0       1.4
          68.0      29.9
          69.0      47.1
          70.0      40.2
          71.0      14.8
          72.0      31.9
          73.0       7.3
          75.0      91.7
          76.0       3.3
          85.0      32.1
          86.0       3.8
         100.0       2.4
         101.0      18.9
         102.0       7.0
         118.0       2.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H15 N O2 0.05 ml : 0.5 ml CDCl3
    4,4-dimethoxybutylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.375 B 3.318 C 2.709 D 1.634 E 1.497 F 1.21

         Hz     ppm     Int.
    

       1754.39   4.390     87
       1748.78   4.376    164
       1743.04   4.362     85
       1326.05   3.319   1000
       1089.60   2.727    121
       1082.64   2.709    194
       1075.44   2.691    128
        665.04   1.665     44
        664.18   1.662     40
        658.20   1.647     90
        652.34   1.633     75
        651.12   1.630     53
        648.68   1.624    107
        643.55   1.611     83
        643.07   1.610     81
        612.43   1.533     41
        611.82   1.531     40
        607.18   1.520     36
        604.74   1.514     79
        603.27   1.510     46
        600.46   1.503     48
        597.17   1.495     82
        596.19   1.492     70
        593.14   1.485     32
        590.33   1.478     59
        588.87   1.474     59
        485.47   1.215     83
    

in CDCl3



liquid film