400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H14 O Si 0.05 ml : 0.5 ml CDCl3 (allyloxy)trimethylsilane 
Assign. Shift(ppm)
A 5.864 B 5.190 C 5.030 D 4.077 E 0.068 J(A,B)=16.8HZ J(A,C)=10.4HZ
Hz ppm Int.2357.30 5.899 31 2346.92 5.873 33 2340.09 5.856 36 2329.83 5.830 37 2083.37 5.213 54 2081.54 5.209 55 2066.28 5.171 48 2064.45 5.166 49 2016.24 5.046 49 2014.65 5.042 47 2005.86 5.020 46 2004.27 5.016 46 1633.54 4.088 70 1631.84 4.084 119 1630.13 4.079 79 1628.54 4.075 78 1626.83 4.071 119 1625.24 4.067 78 31.13 0.078 110 27.34 0.069 1000 24.29 0.061 125
in CDCl3
liquid film
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