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网站主页CAS数据库列表 18031-40-8更多图谱紫苏醛(18031-40-8)核磁图(13CNMR)

紫苏醛

产品名称 紫苏醛

CAS号18031-40-8

分子式C10H14O

分子量150.22

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  • Mass

    MS-NW-7554          
    (S)-(-)-4-isopropenyl-1-cyclohexene-1-carbaldehyde
    C10H14O             (Mass of molecular ion:    150)
    

       Source Temperature: 260 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          15.0       1.1
          18.0       1.2
          26.0       1.3
          27.0      23.1
          28.0       2.3
          29.0      10.6
          38.0       2.1
          39.0      33.8
          40.0       9.8
          41.0      33.5
          42.0       4.7
          43.0       7.0
          50.0       4.4
          51.0      12.4
          52.0       5.7
          53.0      34.1
          54.0       4.9
          55.0      12.9
          56.0       1.2
          57.0       1.3
          58.0       1.5
          59.0       2.0
          62.0       1.3
          63.0       3.9
          64.0       1.0
          65.0       9.6
          66.0       8.5
          67.0      58.4
          68.0     100.0
          69.0       8.4
          70.0       1.0
          74.0       1.0
          75.0       1.1
          77.0      26.6
          78.0       7.1
          79.0      59.8
          80.0      12.9
          81.0      12.3
          82.0       3.6
          83.0       2.2
          89.0       1.1
          90.0       1.0
          91.0      25.2
          92.0       9.7
          93.0      31.0
          94.0      11.7
          95.0      15.2
          96.0       2.4
         103.0       3.3
         104.0       1.8
         105.0      14.2
         106.0      16.9
         107.0      38.8
         108.0      21.0
         109.0       9.8
         110.0       1.2
         115.0       2.6
         117.0       9.3
         118.0       1.2
         119.0       6.4
         120.0       1.5
         121.0      20.7
         122.0      23.9
         123.0       3.1
         131.0       1.7
         132.0       5.2
         133.0       5.3
         134.0       1.7
         135.0      23.3
         136.0       2.9
         145.0       1.8
         146.0       1.8
         148.0       3.5
         149.0       2.3
         150.0      19.8
         151.0       2.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H14 O 0.05 ml : 0.5 ml CDCl3
    (S)-(-)-4-isopropenyl-1-cyclohexene-1-carbaldehyde
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.438 B 6.842 C *1 4.782 D *1 4.738 E 2.47 F 2.26 G *2 2.12 J 1.914 K 1.763 L *2 1.45 ASSIGNED BY H-H COSY.

         Hz     ppm     Int.
    

       3771.97   9.439    608
       2738.65   6.853     90
       2737.43   6.850    149
       2736.33   6.847    158
       2734.62   6.843    141
       2732.42   6.838    148
       2731.45   6.835    144
       2730.10   6.832     94
       2729.00   6.829     82
       1914.43   4.791     82
       1912.96   4.787    236
       1911.25   4.783    359
       1909.79   4.779    290
       1908.33   4.776    113
       1894.65   4.741    300
       1893.80   4.739    332
       1893.07   4.737    299
       1003.30   2.511     52
       1000.61   2.504     50
        991.33   2.481     90
        990.48   2.479     94
        988.77   2.475    131
        987.67   2.472    119
        985.84   2.467    122
        984.50   2.464    113
        983.03   2.460     85
        982.30   2.458     84
        981.32   2.456     84
        980.22   2.453     59
        972.53   2.434     53
        970.70   2.429     78
        969.60   2.427     76
        968.87   2.425     74
        967.65   2.422     90
        966.43   2.419     84
        964.36   2.414     79
        962.52   2.409     49
        911.38   2.281     75
        908.81   2.275    103
        907.23   2.271     89
        906.01   2.268    105
        904.91   2.265     88
        902.47   2.259    134
        901.12   2.255    115
        899.90   2.252    112
        896.00   2.242     63
        892.21   2.233    209
        861.69   2.157     57
        859.38   2.151     61
        855.96   2.142     57
        853.88   2.137     57
        850.46   2.129     51
        848.39   2.123     69
        846.56   2.119     65
        844.36   2.113     57
        841.55   2.106     50
        830.81   2.079     50
        774.78   1.939     57
        772.46   1.933     77
        769.65   1.926     70
        769.29   1.925     71
        767.94   1.922     53
        766.85   1.919     68
        766.24   1.918     67
        763.67   1.911     57
        761.35   1.906     71
        758.54   1.899     76
        755.74   1.892     73
        753.42   1.886     61
        706.30   1.768    780
        704.83   1.764   1000
        703.98   1.762    975
        599.85   1.501     57
        594.48   1.488     66
        588.75   1.474     92
        586.79   1.469     68
        583.37   1.460     90
        581.54   1.456     66
        577.51   1.446     58
        575.56   1.441     79
        572.14   1.432     58
        570.31   1.428     64
    

in CDCl3



liquid film