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网站主页CAS数据库列表 17700-09-3更多图谱2,3,4-三氯硝基苯(17700-09-3)质谱(MS)

2,3,4-三氯硝基苯

产品名称 2,3,4-三氯硝基苯

CAS号17700-09-3

分子式C6H2Cl3NO2

分子量226.44

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  • Mass

    MS-NW-9646          
    1,2,3-trichloro-4-nitrobenzene
    C6H2Cl3NO2          (Mass of molecular ion:    225)
    

       Source Temperature: 270 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       2.0
          28.0       2.8
          30.0      36.3
          35.0       1.2
          36.0       4.0
          37.0       6.1
          38.0       2.6
          47.0       1.9
          48.0       1.0
          49.0       3.8
          50.0       2.9
          54.0       1.4
          60.0       2.0
          61.0       5.4
          62.0       3.8
          71.0       2.2
          72.0       4.5
          73.0      17.2
          74.0      41.7
          75.0       3.9
          83.0       5.5
          84.0      19.6
          85.0       5.9
          86.0       7.0
          87.0       2.5
          88.0       1.1
          96.0       2.4
          97.0       8.5
          98.0       1.7
          99.0       2.8
         106.0       1.2
         107.0       8.7
         108.0      30.1
         109.0      43.3
         110.0      12.6
         111.0      13.5
         112.0       1.0
         118.0       4.8
         119.0       4.3
         120.0       3.3
         121.0       2.8
         122.0       1.0
         125.0       1.2
         131.0       1.3
         132.0       2.0
         133.0       1.0
         134.0       1.4
         143.0      73.7
         144.0      32.1
         145.0      49.6
         146.0      20.7
         147.0       9.1
         148.0       3.4
         158.0       1.2
         160.0       4.1
         162.0       2.6
         167.0      69.6
         168.0       4.0
         169.0      67.5
         170.0       3.7
         171.0      22.0
         172.0       1.3
         173.0       2.4
         178.0       1.1
         179.0      81.2
         180.0       7.0
         181.0      78.9
         182.0       6.1
         183.0      25.2
         184.0       1.9
         185.0       2.8
         195.0      57.7
         196.0       3.9
         197.0      55.4
         198.0       3.8
         199.0      18.4
         200.0       1.2
         201.0       2.0
         209.0       4.0
         211.0       3.8
         213.0       1.3
         225.0     100.0
         226.0       7.0
         227.0      96.3
         228.0       6.8
         229.0      31.4
         230.0       2.3
         231.0       3.5
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H2 Cl3 N O2 0.036 g : 0.5 ml CDCl3
    1,2,3-trichloro-4-nitrobenzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.681 B 7.560 J(A,B)=8.8HZ

         Hz     ppm     Int.
    

        694.81   7.759    222
        688.81   7.692     33
        686.00   7.660    785
        683.31   7.630     61
        682.56   7.622     57
        682.00   7.616     57
        681.69   7.612     58
        679.38   7.586   1000
        677.56   7.566     77
        675.69   7.545     42
        674.44   7.531     40
        673.94   7.526     32
        672.50   7.509     32
        670.56   7.488    300
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder