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网站主页CAS数据库列表 1476-98-8更多图谱氢鲲盐酸盐(1476-98-8)红外图谱(IR2)

氢鲲盐酸盐

产品名称 氢鲲盐酸盐

CAS号1476-98-8

分子式C20H27ClN2O2

分子量362.89

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  • Mass

    MS-NW-8996          
    hydroquinidine hydrochloride
    C20H26N2O2 HCl      (Mass of molecular ion:    326)
    

       Source Temperature: 260 °C
       Sample Temperature: 220 °C
       Direct, 75 eV
    

          18.0       1.7
          28.0       1.6
          29.0       2.1
          30.0       1.7
          36.0      13.1
          38.0       4.3
          41.0       8.1
          42.0       5.8
          43.0       2.0
          44.0       2.6
          53.0       1.1
          54.0       1.3
          55.0      21.3
          56.0       7.7
          57.0       1.3
          67.0       3.1
          68.0       2.3
          69.0       3.4
          70.0       5.3
          77.0       1.0
          79.0       1.0
          80.0       1.1
          81.0       1.9
          82.0      40.3
          83.0       8.6
          84.0       3.8
          94.0       1.5
          95.0       4.0
          96.0       3.3
          97.0       1.5
         108.0       2.0
         109.0       1.8
         110.0      35.1
         111.0       6.5
         112.0       1.2
         116.0       1.6
         117.0       3.4
         122.0       1.3
         123.0       1.6
         124.0       3.5
         125.0       1.5
         126.0      11.6
         127.0       1.3
         128.0       1.0
         130.0       1.0
         136.0       1.4
         138.0     100.0
         139.0      48.8
         140.0       9.1
         141.0       1.0
         145.0       2.4
         146.0       1.0
         151.0       1.1
         152.0       7.8
         153.0       1.0
         154.0       1.8
         154.5       1.0
         158.0       4.3
         159.0       4.3
         160.0      13.3
         161.0       1.7
         166.0       1.1
         168.0       3.7
         169.0       1.4
         170.0       1.3
         172.0       7.7
         173.0      14.4
         174.0       6.8
         175.0       1.1
         176.0       1.5
         183.0       1.1
         184.0       2.2
         185.0       1.3
         186.0       4.8
         187.0       3.4
         188.0       6.0
         189.0      26.4
         190.0       3.5
         196.0       2.2
         197.0       1.0
         198.0       2.3
         199.0       2.2
         200.0       2.8
         201.0      11.0
         202.0       3.6
         211.0       1.0
         212.0       1.2
         213.0       1.4
         214.0       3.4
         215.0       1.5
         222.0       1.0
         224.0       1.9
         225.0       1.0
         226.0       1.2
         227.0       1.3
         240.0       1.1
         241.0       1.0
         243.0       1.1
         251.0       1.1
         252.0       6.7
         253.0       1.8
         267.0       2.6
         268.0       1.3
         269.0       6.9
         270.0       1.7
         279.0       1.5
         281.0       1.4
         283.0       1.4
         285.0       5.3
         286.0       1.0
         295.0       1.3
         297.0      17.5
         298.0       4.0
         308.0       1.5
         309.0       5.2
         310.0       2.3
         311.0      14.7
         312.0       3.2
         324.0       1.6
         325.0       4.1
         326.0      81.1
         327.0      20.8
         328.0       2.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C20 H26 N2 O2 0.037 g : 0.5 ml CDCl3
    hydroquinidine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 11.7 B 8.665 C 7.692 D 7.626 E 6.896 F 6.774 G 6.507 J 6.442 K *1 4.229 L 3.513 M *1 3.32 N 3.217 P *1 3.062 Q *2 3.390 R 1.932 S *3 1.78 T *3 1.65 U 0.953 V *2 0.93

         Hz     ppm     Int.
    

       3465.33   8.671    133
       3460.75   8.660    139
       3076.28   7.698    137
       3071.89   7.687    133
       3052.84   7.639    167
       3043.68   7.616    179
       2762.15   6.912     94
       2759.59   6.906    105
       2752.99   6.889     89
       2750.43   6.883    100
       2708.85   6.779    139
       2706.28   6.772    127
       2602.61   6.513     74
       2599.13   6.504     99
       2576.42   6.447    105
       2572.21   6.437     80
       1700.33   4.255     30
       1691.91   4.234     36
       1689.71   4.228     39
       1688.25   4.225     36
       1687.51   4.223     36
       1680.92   4.206     33
       1679.45   4.203     33
       1404.34   3.514   1000
       1344.99   3.366     37
       1344.63   3.365     37
       1332.35   3.334     59
       1331.99   3.333     59
       1321.73   3.308     51
       1317.52   3.297     50
       1316.60   3.295     50
       1316.23   3.294     50
       1315.87   3.293     50
       1295.54   3.242     37
       1286.01   3.218     76
       1276.49   3.195     38
       1229.23   3.076     42
       1217.87   3.048     38
        956.68   2.394     38
        955.03   2.390     42
        953.75   2.387     40
        953.38   2.386     40
        771.86   1.932     73
        723.14   1.810     45
        719.29   1.800     54
        718.75   1.799     54
        710.32   1.778     66
        702.63   1.759     45
        702.26   1.758     45
        701.89   1.757     44
        697.86   1.747     38
        690.90   1.729     42
        684.49   1.713     54
        677.35   1.695     82
        669.84   1.677     70
        666.18   1.667     49
        660.86   1.654     54
        657.02   1.644     47
        654.09   1.637     86
        646.76   1.619     63
        388.13   0.972    217
        380.80   0.953    444
        373.66   0.935    198
        368.16   0.922     55
        363.77   0.911     31
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder