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MassMS-NW-5615 1-methyl-3-pyrrolidinol C5H11NO (Mass of molecular ion: 101)
Source Temperature: 280 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 6.4 17.0 2.1 18.0 10.2 26.0 1.4 27.0 5.0 28.0 5.1 29.0 2.6 30.0 2.6 31.0 1.7 39.0 4.3 40.0 1.7 41.0 6.4 42.0 53.7 43.0 6.8 44.0 17.8 53.0 2.0 54.0 1.7 55.0 3.3 56.0 1.9 57.0 100.0 58.0 6.4 67.0 2.5 71.0 1.4 80.0 4.0 81.0 6.3 82.0 10.9 83.0 5.1 84.0 1.3 100.0 5.4 101.0 31.2 102.0 2.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C5 H11 N O 0.05 ml : 0.5 ml CDCl3 1-methyl-3-pyrrolidinol 
Assign. Shift(ppm)
A 4.7 B 4.329 C *1 2.801 D *2 2.58 E *2 2.57 F 2.327 G *3 2.31 J *3 2.199 K *1 1.717
Hz ppm Int.1736.21 4.345 43 1735.23 4.342 36 1732.18 4.335 63 1728.52 4.326 63 1725.46 4.318 39 1723.88 4.314 43 1131.10 2.831 46 1125.98 2.818 49 1122.80 2.810 62 1121.95 2.808 63 1117.80 2.797 61 1116.70 2.795 66 1113.77 2.787 58 1108.76 2.775 56 1032.47 2.584 373 1028.81 2.575 173 1027.47 2.571 237 934.81 2.340 85 930.30 2.328 1000 926.51 2.319 116 925.54 2.316 90 919.80 2.302 88 918.95 2.300 77 917.11 2.295 84 910.64 2.279 69 895.63 2.242 37 890.63 2.229 36 888.06 2.223 40 887.45 2.221 35 882.32 2.208 70 879.88 2.202 30 877.08 2.195 43 874.63 2.189 65 869.38 2.176 46 866.33 2.168 30 701.05 1.755 30 694.46 1.738 33 693.12 1.735 38 691.41 1.731 33 690.19 1.727 35 687.74 1.721 33 686.52 1.718 35 684.69 1.714 32 683.59 1.711 31 681.15 1.705 30 679.69 1.701 32
in CDCl3
liquid film
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