图谱信息 供应商 相关产品
网站主页CAS数据库列表 1128-54-7更多图谱3-甲基-1-苯基吡啶(1128-54-7)质谱(MS)

3-甲基-1-苯基吡啶

产品名称 3-甲基-1-苯基吡啶

CAS号1128-54-7

分子式C10H10N2

分子量158.2

展开


  • Mass

    MS-IW-0984          
    3-methyl-1-phenylpyrazole
    C10H10N2            (Mass of molecular ion:    158)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          39.0       1.5
          50.0       1.3
          51.0       7.8
          52.0       1.3
          54.0       1.2
          55.0       2.2
          63.0       1.5
          64.0       1.5
          65.0       1.2
          77.0      20.1
          78.0       3.3
          79.0       2.2
          81.0       2.5
          89.0       3.9
          90.0       8.8
          91.0       2.3
         103.0       1.3
         104.0       3.1
         115.0       1.0
         116.0       3.1
         117.0       5.0
         118.0       1.8
         129.0       1.1
         130.0      17.0
         131.0       2.7
         132.0       1.2
         142.0       1.9
         143.0       1.7
         156.0       2.6
         157.0      47.9
         158.0     100.0
         159.0      11.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H10 N2 0.037 g : 0.5 ml CDCl3
    3-methyl-1-phenylpyrazole
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.789 B 7.636 C 7.405 D 7.230 E 6.226 F 2.373

         Hz     ppm     Int.
    

       3114.26   7.793    170
       3111.94   7.787    174
       3057.62   7.651    175
       3056.40   7.648    217
       3054.44   7.643     69
       3050.78   7.634     75
       3049.93   7.632    126
       3048.83   7.629    234
       3047.85   7.627    226
       3045.65   7.621     39
       2969.73   7.431     38
       2967.90   7.427    161
       2965.70   7.421     64
       2962.40   7.413     45
       2960.45   7.408    220
       2959.47   7.406    183
       2953.74   7.391     68
       2951.78   7.386    177
       2949.83   7.382     33
       2895.87   7.247     66
       2894.65   7.243     99
       2893.55   7.241     59
       2888.79   7.229     54
       2887.33   7.225    145
       2885.86   7.221     55
       2880.98   7.209     39
       2879.88   7.207     67
       2878.78   7.204     40
       2489.75   6.230    165
       2487.30   6.224    167
        948.49   2.374   1000
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder