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4-(甲硫基)苯酚

产品名称 4-(甲硫基)苯酚

CAS号1073-72-9

分子式C7H8OS

分子量140.2

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  • Mass

    MS-NW-4786          
    p-(methylthio)phenol
    C7H8OS              (Mass of molecular ion:    140)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       1.4
          27.0       2.9
          37.0       1.1
          38.0       2.4
          39.0      11.2
          45.0      15.4
          47.0       1.4
          50.0       1.7
          51.0       2.5
          53.0       8.4
          55.0       1.9
          61.0       1.2
          62.0       2.1
          63.0       5.0
          64.0       1.7
          65.0       5.7
          66.0       1.7
          67.0       1.5
          69.0       5.8
          70.0       4.9
          71.0       2.4
          77.0       2.6
          78.0       1.2
          81.0      12.6
          85.0       1.4
          94.0       4.1
          95.0       2.2
          96.0       2.4
          97.0      18.0
          98.0       1.6
         107.0       2.4
         111.0       1.8
         124.0       1.2
         125.0      84.9
         126.0       6.6
         127.0       4.3
         139.0       2.5
         140.0     100.0
         141.0       8.8
         142.0       4.8
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H8 O S 0.019 g : 0.5 ml CDCl3
    p-(methylthio)phenol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.217 B 6.781 C 4.5 D 2.433

         Hz     ppm     Int.
    

        651.38   7.274    133
        649.56   7.253     74
        644.88   7.201     47
        642.56   7.175    201
        639.69   7.143     25
        610.94   6.822    204
        608.69   6.797     51
        604.38   6.749     41
        602.13   6.724    129
        217.88   2.433   1000
    


  • 1H NMR 399.65 MHz
    C7 H8 O S 0.017 g : 0.5 ml CDCl3
    p-(methylthio)phenol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.222 B 6.787 C 5. D 2.439

         Hz     ppm     Int.
    

       2890.99   7.234    172
       2888.79   7.229     58
       2884.40   7.218     55
       2882.20   7.212    189
       2879.15   7.205     25
       2716.92   6.799    196
       2714.72   6.793     61
       2710.33   6.782     54
       2708.13   6.777    174
       2705.08   6.769     22
        974.61   2.439   1000
        971.07   2.430     31
    

in CDCl3



CCl4 solution



KBr disc



nujol mull