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网站主页CAS数据库列表 105-81-7更多图谱N-(2-羟乙基)-N’-2-丙烯基硫脲(105-81-7)红外图谱(IR1)

N-(2-羟乙基)-N’-2-丙烯基硫脲

产品名称 N-(2-羟乙基)-N’-2-丙烯基硫脲

CAS号105-81-7

分子式C6H12N2OS

分子量160.24

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  • Mass

    MS-NW-0208          
    1-allyl-3-(2-hydroxyethyl)thiourea
    C6H12N2OS           (Mass of molecular ion:    160)
    

       Source Temperature: 220 °C
       Sample Temperature:   0 °C
       Direct, 75 eV
    

          15.0       5.7
          18.0       3.6
          19.0       2.9
          26.0       2.2
          27.0      12.6
          28.0      31.5
          29.0       4.8
          30.0      59.1
          31.0       6.9
          32.0       1.4
          33.0       1.1
          34.0       1.8
          38.0       2.2
          39.0      31.7
          40.0       3.2
          41.0     100.0
          42.0      15.8
          43.0      28.5
          44.0      15.6
          45.0      18.3
          46.0       2.1
          47.0       2.2
          52.0       1.2
          54.0       7.8
          55.0       8.4
          56.0      74.3
          57.0      50.7
          58.0      11.0
          59.0       8.5
          60.0      30.0
          61.0       3.1
          62.0       7.0
          67.0       2.7
          68.0       3.7
          69.0       7.1
          70.0       2.6
          71.0       2.4
          72.0       7.4
          73.0       8.5
          74.0       8.8
          75.0       2.5
          76.0       1.0
          77.0       4.2
          81.0       2.2
          82.0       2.2
          83.0      17.8
          84.0       2.3
          85.0       1.5
          86.0      17.3
          87.0       3.2
          88.0       2.0
          90.0       1.5
          95.0       2.1
          98.0       2.0
          99.0       3.5
         100.0       9.9
         101.0      32.5
         102.0       2.4
         103.0       3.2
         104.0       3.5
         109.0       1.1
         113.0       2.5
         114.0       3.3
         115.0      12.6
         116.0       3.2
         117.0       3.2
         125.0       2.2
         126.0       2.0
         127.0       8.4
         129.0       3.8
         131.0       1.0
         141.0       4.0
         142.0       5.0
         143.0       1.8
         145.0      80.1
         146.0       5.7
         147.0       4.1
         159.0       3.4
         160.0      97.2
         161.0       9.1
         162.0       5.1
    

400 MHz in DMSO-d6

90 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C6 H12 N2 O S 0.040 g : 0.5 ml DMSO-d6
    1-allyl-3-(2-hydroxyethyl)thiourea
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 7.60 B *1 7.44 C 5.837 D 5.146 E 5.071 F 4.77 G 4.05 J 3.48 SIGNAL J OVERLAPPED BY THE IMPURITY PEAK.

         Hz     ppm     Int.
    

       3038.82   7.604    184
       2974.37   7.443    243
       2348.63   5.877    166
       2343.63   5.865    173
       2338.26   5.851    213
       2337.16   5.849    179
       2331.54   5.834    241
       2326.29   5.821    210
       2321.17   5.809    221
       2065.92   5.170    394
       2064.33   5.166    434
       2062.62   5.162    256
       2048.71   5.127    376
       2047.12   5.123    421
       2045.53   5.119    265
       2032.59   5.086    432
       2031.01   5.082    456
       2022.34   5.061    401
       2020.75   5.057    412
       1907.96   4.775    203
       1617.92   4.049    372
       1394.29   3.489    760
       1389.40   3.477   1000
       1367.80   3.423    219
    


  • 1H NMR 89.56 MHz
    C6 H12 N2 O S 0.048 g : 0.5 ml DMSO-d6
    1-allyl-3-(2-hydroxyethyl)thiourea
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.5 B 7.4 C 5.85 D 5.13 E 5.09 F 4.74 G 4.045 J 3.44

         Hz     ppm     Int.
    

        679.25   7.585    160
        663.94   7.414    157
        543.63   6.071     66
        538.31   6.011    127
        533.56   5.958    105
        528.44   5.901    154
        526.25   5.876     98
        523.31   5.844     81
        521.00   5.818    205
        516.31   5.765    168
        511.06   5.707    255
        505.94   5.650    135
        471.25   5.262    104
        469.50   5.243    300
        467.56   5.221    408
        465.94   5.203    171
        460.94   5.147    170
        459.44   5.130    378
        457.94   5.114    242
        457.44   5.108    237
        456.00   5.092    106
        453.88   5.068     96
        452.19   5.050    232
        450.19   5.027    317
        449.50   5.019    324
        448.63   5.010    226
        448.00   5.003    219
        447.56   4.998    222
        446.00   4.980     99
        424.19   4.737    253
        367.75   4.107    272
        366.25   4.090    186
        362.38   4.047    475
        358.31   4.001    191
        357.00   3.987    245
        355.50   3.970    134
        310.44   3.467   1000
    

KBr disc



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