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网站主页CAS数据库列表 101-79-1更多图谱4'-氯-4-氨基二苯醚(101-79-1)质谱(MS)

4'-氯-4-氨基二苯醚

产品名称 4'-氯-4-氨基二苯醚

CAS号101-79-1

分子式C12H10ClNO

分子量219.67

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  • Mass

    MS-NW-7928          
    p-(p-chlorophenoxy)aniline
    C12H10ClNO          (Mass of molecular ion:    219)
    

       Source Temperature: 150 °C
       Sample Temperature:  90 °C
       Direct, 75 eV
    

          18.0       1.0
          27.0       1.5
          28.0       2.5
          38.0       1.4
          39.0       5.8
          41.0       1.4
          50.0       2.8
          51.0       2.5
          52.0       3.3
          53.0       5.2
          54.0       1.7
          62.0       1.0
          63.0       3.5
          64.0       2.3
          65.0       9.6
          66.0       1.5
          74.0       1.3
          75.0       5.4
          76.0       1.2
          77.0       1.3
          80.0      13.2
          81.0       1.1
          92.0       2.0
         108.0      78.6
         109.0       6.2
         111.0       3.0
         113.0       1.0
         127.0       1.8
         128.0       2.2
         139.0       1.0
         154.0       1.5
         156.0       6.1
         183.0       1.4
         184.0       1.0
         190.0       3.3
         192.0       1.2
         218.0       1.8
         219.0     100.0
         220.0      14.5
         221.0      32.8
         222.0       4.5
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C12 H10 Cl N O 0.036 g : 0.5 ml DMSO-d6
    p-(p-chlorophenoxy)aniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.333 B 6.870 C 6.782 D 6.618 E 5.04

         Hz     ppm     Int.
    

       2938.84   7.354    111
       2935.30   7.345    875
       2933.23   7.340    303
       2928.71   7.329    319
       2926.51   7.323    994
       2922.97   7.314    103
       2753.42   6.890    131
       2750.00   6.882    958
       2747.80   6.876    313
       2743.16   6.864    305
       2741.09   6.859    895
       2737.43   6.850     92
       2718.63   6.803    104
       2715.21   6.794    786
       2713.13   6.789    278
       2708.74   6.778    317
       2706.54   6.773   1000
       2703.13   6.764    111
       2652.22   6.637    138
       2648.80   6.628    992
       2646.73   6.623    303
       2642.33   6.612    278
       2640.14   6.607    778
       2636.72   6.598     78
       2013.18   5.038    676
    

in DMSO-d6

in CDCl3





KBr disc



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