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网站主页CAS数据库列表 100-69-6更多图谱2-乙烯基吡啶(100-69-6)质谱(MS)

2-乙烯基吡啶

产品名称 2-乙烯基吡啶

CAS号100-69-6

分子式C7H7N

分子量105.14

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  • Mass

    MS-NW-0763          
    2-vinylpyridine
    C7H7N               (Mass of molecular ion:    105)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          26.0       2.5
          27.0       4.1
          28.0       2.4
          37.0       1.7
          38.0       2.4
          39.0       4.7
          49.0       1.2
          50.0      10.7
          51.0      20.1
          52.0      22.4
          52.5       3.1
          53.0       3.1
          63.0       1.8
          74.0       1.9
          75.0       1.8
          76.0       2.6
          77.0       6.6
          78.0      16.0
          79.0      79.6
          80.0       4.8
         104.0      55.0
         105.0     100.0
         106.0       9.3
         107.0       1.0
         118.0       1.1
    

parameter in CCl4


  • 1H NMR 300 MHz
    C7 H7 N 15 wt% in CCl4
    2-vinylpyridine
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 8.470 D(B) 6.996 D(C) 7.477 D(D) 7.165 D(E) 6.712 D(F) 5.368 D(G) 6.205 J(A,B) 4.79 J(A,C) 1.87 J(A,D) 1.01 J(A,E) 0.24 J(A,F) 0.0 J(A,G) 0.0 J(B,C) 7.54 J(B,D) 1.15 J(B,E) -0.24 J(B,F) 0.22 J(B,G) 0.22 J(C,D) 7.83 J(C,E) 0.25 J(C,F) 0.03 J(C,G) 0.03 J(D,E) -0.25 J(D,F) 0.24 J(D,G) 0.07 J(E,F) 10.77 J(E,G) 17.44 J(F,G) 1.66 ROWBOTHAM,J.B. & SCHAEFER,T. CAN.J.CHEM. 52, 136 (1974) J(C,F):LESS THAN 0.03HZ. J(C,G):LESS THAN 0.03HZ. J(D,G):LESS THAN 0.07HZ.

         Hz     ppm     Int.
    

       2544.81   8.483    495
       2543.84   8.479    578
       2543.01   8.477    585
       2542.02   8.473    534
       2540.05   8.467    530
       2539.05   8.463    596
       2538.23   8.461    592
       2537.23   8.457    521
       2251.99   7.507    379
       2250.11   7.500    378
       2244.30   7.481    795
       2242.42   7.475    787
       2236.64   7.455    498
       2234.76   7.449    490
       2154.26   7.181    555
       2153.26   7.178    943
       2152.26   7.174    579
       2146.42   7.155    476
       2145.45   7.151    801
       2144.42   7.148    482
       2105.41   7.018    468
       2104.32   7.014    459
       2100.59   7.002    475
       2099.50   6.998    478
       2097.89   6.993    460
       2096.80   6.989    423
       2093.10   6.977    419
       2091.99   6.973    401
       2028.25   6.761    620
       2017.54   6.725    648
       2010.81   6.703    778
       2000.10   6.667    815
       1870.57   6.235    991
       1868.90   6.230   1000
       1853.13   6.177    796
       1851.46   6.172    788
       1616.54   5.388    878
       1614.86   5.383    857
       1605.82   5.353    822
       1604.15   5.347    811
    

in CDCl3



liquid film