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网站主页CAS数据库列表 100-64-1更多图谱环己酮肟(100-64-1)核磁图(13CNMR)

环己酮肟

产品名称 环己酮肟

CAS号100-64-1

分子式C6H11NO

分子量113.16

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  • Mass

    MS-NW-1838          
    cyclohexanone oxime
    C6H11NO             (Mass of molecular ion:    113)
    

       Source Temperature: 240 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       4.4
          18.0       3.6
          26.0       7.5
          27.0      46.8
          28.0      24.7
          29.0      26.6
          30.0       9.5
          31.0       3.7
          37.0       2.1
          38.0       5.5
          39.0      52.2
          40.0      14.4
          41.0     100.0
          42.0      42.7
          43.0       7.4
          44.0       9.1
          45.0       2.2
          46.0      14.7
          50.0       3.9
          51.0       7.2
          52.0       6.4
          53.0      20.5
          54.0      49.5
          55.0      69.1
          56.0       7.8
          57.0       7.1
          58.0       1.7
          59.0      57.0
          60.0       1.7
          63.0       1.2
          64.0       1.2
          65.0       4.0
          66.0       5.5
          67.0      37.8
          68.0      37.2
          69.0      22.8
          70.0       6.0
          71.0       1.8
          72.0      45.2
          73.0       2.1
          77.0       2.8
          79.0      10.6
          80.0       6.8
          81.0      27.3
          82.0       5.6
          83.0       2.5
          84.0      14.7
          85.0      22.2
          86.0       1.5
          94.0       3.9
          95.0       1.2
          96.0      19.7
          97.0       4.5
          98.0      22.3
          99.0       1.4
         112.0       3.6
         113.0      70.3
         114.0       5.4
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H11 N O 0.044 g : 0.5 ml CDCl3
    cyclohexanone oxime
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.9 B 2.50 C 2.22 D 1.74 to 1.55

         Hz     ppm     Int.
    

        798.00   8.911     50
        230.94   2.579    104
        228.19   2.548    148
        225.00   2.513    283
        220.50   2.463    159
        219.25   2.449    196
        205.06   2.290    107
        199.56   2.229    261
        199.06   2.223    257
        195.69   2.186    149
        193.31   2.159    219
        189.88   2.121     42
        160.81   1.796     42
        160.38   1.791     41
        158.13   1.766     61
        156.00   1.742    116
        151.69   1.694    250
        145.75   1.628   1000
        143.75   1.606    923
        142.19   1.588    512
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder