parameter in TMS+OCTAFLUOROCYCLOBUTANE
-
1H NMR 300 MHz C6 H3 F3 70 vol% in trifluorobenzene 1,2,4-trifluorobenzene Parameter ppm Hz
D(A) 6.807 D(B) 6.715 D(C) 7.019 D(X) -9.164 D(Y) 7.234 D(Z) 18.760 J(A,B) 3.05 J(A,C) 0.37 J(A,X) 6.31 J(A,Y) 10.54 J(A,Z) 8.32 J(B,C) 9.23 J(B,X) 3.27 J(B,Y) -2.03 J(B,Z) 7.77 J(C,X) 9.94 J(C,Y) 8.88 J(C,Z) 5.07 J(X,Y) -20.01 J(X,Z) 15.04 J(Y,Z) 3.14 LUSTIG,E. ET AL. J.CHEM.PHYS. 51, 1839 (1969) F-19 REFERENCE : OCTAFLUOROCYCLOBUTANE
Hz ppm Int.
2122.46 7.075 380 2117.18 7.057 441 2113.22 7.044 1000 2108.10 7.027 912 2103.74 7.012 958 2098.80 6.996 863 2094.43 6.981 529 2089.35 6.964 515 2056.24 6.854 391 2053.25 6.844 473 2049.93 6.833 476 2047.78 6.826 553 2046.89 6.823 622 2045.51 6.818 622 2045.04 6.817 608 2042.52 6.808 544 2041.68 6.806 545 2039.33 6.798 589 2038.63 6.795 601 2037.29 6.791 586 2036.40 6.788 611 2034.32 6.781 474 2031.10 6.770 466 2028.00 6.760 559 2027.24 6.757 395 2024.81 6.749 436 2024.06 6.747 483 2021.71 6.739 606 2020.61 6.735 418 2019.38 6.731 411 2018.57 6.729 480 2017.93 6.726 497 2017.43 6.725 479 2015.79 6.719 718 2014.29 6.714 914 2012.63 6.709 716 2011.15 6.704 558 2010.19 6.701 413 2009.33 6.698 342 2008.14 6.694 368 2007.07 6.690 421 2006.62 6.689 416 2004.99 6.683 536 2003.53 6.678 265 2001.83 6.673 289
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