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MassMS-NW-1002 N-sulfinylaniline C6H5NOS (Mass of molecular ion: 139)
Source Temperature: 260 °C Sample Temperature: 130 °C Reservoir, 75 eV
18.0 1.7 26.0 1.4 27.0 3.2 28.0 3.8 32.0 1.3 37.0 5.4 38.0 10.9 39.0 15.9 40.0 2.7 41.0 5.7 45.0 18.0 46.0 1.1 48.0 5.0 50.0 6.3 51.0 14.0 52.0 6.3 53.0 2.3 55.5 1.7 58.0 2.2 61.0 2.4 62.0 4.0 63.0 17.6 64.0 33.5 65.0 18.3 66.0 4.9 67.0 21.3 68.0 1.1 74.0 1.4 75.0 1.0 76.0 1.0 77.0 7.6 78.0 7.1 79.0 1.0 84.0 25.2 85.0 3.3 86.0 1.7 90.0 3.7 91.0 24.6 92.0 3.3 93.0 13.2 94.0 1.0 96.0 1.0 106.0 1.6 110.0 16.7 111.0 35.0 112.0 6.8 113.0 1.9 122.0 2.3 123.0 1.3 138.0 6.1 139.0 100.0 140.0 8.2 141.0 4.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H5 N O S 0.02 ml : 0.5 ml CDCl3 N-sulfinylaniline 
Assign. Shift(ppm)
A 7.849 B 7.30 to 7.51
Hz ppm Int.708.44 7.911 350 704.75 7.870 446 703.25 7.853 306 701.06 7.828 466 700.00 7.816 269 698.56 7.800 578 669.31 7.474 200 666.38 7.441 600 665.63 7.433 490 664.19 7.417 321 662.44 7.397 657 661.31 7.384 316 659.63 7.366 1000 658.63 7.355 257 658.25 7.350 256
in CDCl3
liquid film
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