2-BROMO-N-(3,5-DIMETHYL-PHENYL)-ACETAMIDE

Preparation

10 ml freshly prepared solution of 10 % sodium carbonate was added in a clean round bottom flask rinsed with distilled water followed by the addition of 0.1 ml of 3,5-dimethyl aniline. Mix it properly and 1 ml of acid was added safely with the help of pipette into the flask. Shake it well so that precipitates appeared. Filter the ppts by using filter paper and wash the product with distilled water properly. Dry the ppts, collect them, weigh them and save.