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4-ACETAMIDO-TEMPO

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4-ACETAMIDO-TEMPO Usage And Synthesis
  • Chemical PropertiesORANGE-RED CRYSTALLINE POWDER
  • Purification MethodsDissolve the 1-oxyl in CH2Cl2, wash it with saturated K2CO3, then saturated aqueous NaCl, dry (Na2SO4), filter and evaporate. The red solid is recrystallised from aqueous MeOH, m 147.5o. [Ma & Bobbitt J Org Chem 56 6110 1991, Rozantsev & Kokhanov Bull Acad Sci USSR, Div Chem Sci 15 1422 1966, Beilstein 22/8 V 174.]
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