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1-Iodopropane

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1-Iodopropane Basic information
1-Iodopropane Chemical Properties
  • Melting point:-101 °C
  • Boiling point:101-102 °C(lit.)
  • Density 1.743 g/mL at 25 °C(lit.)
  • vapor pressure 43 mm Hg ( 25 °C)
  • refractive index n20/D 1.504(lit.)
  • Flash point:112 °F
  • storage temp. Flammables area
  • solubility 1.1g/l
  • form Liquid
  • color Clear colorless to yellow
  • Water Solubility Fully miscible in water.
  • Sensitive Light Sensitive
  • Merck 14,7862
  • BRN 505937
  • Henry's Law Constant(x 10-3 atm?m3/mol): 9.09 at 25 °C (Hine and Mookerjee, 1975)
  • Stability:Stable, but may discolour on exposure to light. Incompatible with strong oxidizing agents, strong bases. Flammable.
  • CAS DataBase Reference107-08-4(CAS DataBase Reference)
  • NIST Chemistry ReferencePropane, 1-iodo-(107-08-4)
  • EPA Substance Registry SystemPropane, 1-iodo- (107-08-4)
Safety Information
  • Hazard Codes Xn,Xi,N
  • Risk Statements 10-20-36/37/38-52/53-2017/10/20
  • Safety Statements 16-26-36/37-61
  • RIDADR UN 2392 3/PG 3
  • WGK Germany 3
  • RTECS TZ4100000
  • 8
  • Hazard Note Irritant
  • TSCA Yes
  • HazardClass 3
  • PackingGroup III
  • HS Code 29033080
  • ToxicityLD50 (inhalation) for rats 73,000 mg/m3/30-min (quoted, RTECS, 1985).
MSDS
1-Iodopropane Usage And Synthesis
  • Chemical Propertiescolourless liquid
  • Physical propertiesClear, colorless liquid with a characteristic sharp, penetrating odor. On exposure to light, 1- iodopropane may become pale yellow.
  • Synthesis Reference(s)Tetrahedron Letters, 8, p. 4131, 1967 DOI: 10.1016/S0040-4039(01)89706-9
  • Environmental FateBiological. A strain of Acinetobacter sp. isolated from activated sludge degraded 1-iodopropane to 1-propanol and iodide ions (Janssen et al., 1987).
    Chemical/Physical. Slowly hydrolyzes in water forming 1-propanol and hydroiodic acid.
  • Purification MethodsIt should be distilled first under reduced pressure to avoid decomposition. Dry the iodide with MgSO4 or silica gel and fractionally distil it. Store it under nitrogen with mercury in a brown bottle. Prior to distillation, free iodine can be removed by shaking with copper powder or by washing with aqueous Na2S2O3 and drying. Alternatively, the n-propyl iodide can be treated with bromine, then washed with aqueous Na2S2O3, dried and distilled. See also n-butyl iodide. [Beilstein 1 IV 222.]
1-Iodopropane Preparation Products And Raw materials
1-Iodopropane(107-08-4)Related Product Information
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