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Ferrocenecarboxylic acid

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Ferrocenecarboxylic acid Basic information
Ferrocenecarboxylic acid Chemical Properties
Safety Information
  • Hazard Codes Xn
  • Risk Statements 36/37/38-22
  • Safety Statements 37/39-26
  • WGK Germany 3
  • HS Code 29319090
MSDS
Ferrocenecarboxylic acid Usage And Synthesis
  • Chemical Propertiesdark brown powder
  • UsesFerrocenecarboxylic acid is used to esterify complex mixtures of phenols and alcohols for analysis by GCMS.
  • Purification MethodsIt crystallises as yellow crystals from pet ether (m 225-230odec), CHCl3 (m 208.5odec), toluene/pet ether (m 195-205odec), or aqueous ethanol. [Matsue et al. J Am Chem Soc 107 3411 1985.] The acid chloride m 49o crystallises from pentane, and has max at 458nm [Lau & Hart J Org Chem 24 280 1959]. The methyl ester crystallises from aqueous MeOH with m 70-71o. The anhydride has m 143-145o when recrystallised from pet ether [Acton & Silverstein J Org Chem 24 1487 1959]. The amide has m 168-170o when crystallised from CHCl3/Et2O or m 167-169o when crystallised from *C6H6/MeOH. [Arimoto & Haven J Am Chem Soc 77 6295 1955, Benkeser et al. J Am Chem Soc 76 4025 1954.] [Beilstein 16 IV 1807.]
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