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Acetamidine hydrochloride

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Acetamidine hydrochloride Basic information
Acetamidine hydrochloride Chemical Properties
  • Melting point:165-170 °C(lit.)
  • Boiling point:129.78°C (rough estimate)
  • Density 1.0596 (rough estimate)
  • refractive index 1.5500 (estimate)
  • pkapK1: 1.60(+1) (25°C)
  • form Crystalline Powder, Crystals and/or Chunks
  • color White to cream
  • Water Solubility 1 g/mL
  • Sensitive Hygroscopic
  • Merck 14,44
  • BRN 3591762
  • InChIKeyWCQOBLXWLRDEQA-UHFFFAOYSA-N
  • CAS DataBase Reference124-42-5(CAS DataBase Reference)
  • EPA Substance Registry SystemEthanimidamide, monohydrochloride (124-42-5)
Safety Information
  • Hazard Codes Xi
  • Risk Statements 36/37/38-36/38
  • Safety Statements 26-37/39
  • WGK Germany 3
  • 3
  • TSCA Yes
  • HS Code 29252000
MSDS
Acetamidine hydrochloride Usage And Synthesis
  • Chemical PropertiesWHITE FINE CRYSTALLINE POWDER
  • Purification MethodsThe hydrochlorde can be recrystallised from small volumes of EtOH. Alternatively it is dissolved in EtOH, filtered, Et2O is added; filter the crystalline salt off under N2 and dry it in a vacuum desiccator over H2SO4. The salt is deliquescent and should be stored in a tightly stoppered container. Its solubility in H2O is 10% at room temperature and it is soluble in Me2CO. The free base reacts strongly alkaline in H2O. It has max 224nm ( 4000) in H2O. The picrate has m 252o (sintering at ~245o). [Dox Org Synth Coll Vol I 5 1941, Davies & Parsons Chem Ind (London) 628 1958, Barnes et al. J Am Chem Soc 62 1286 1940 give m 177-178o, Beilstein 2 H 185, 2 I 85, 2 II 183, 2 III 416, 2 IV 428.]
Acetamidine hydrochloride Preparation Products And Raw materials
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