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DIPHENYLCARBAZONE

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It crystallises from EtOH (ca 5mL/g), and dry the orange-red needles at 50o. A commercial sample, nominally sym-diphenylcarbazone (m 154-156o) was a mixture of diphenylcarbazide and diphenylcarbazone. The former was removed by dissolving 5g of the crude material in 75mL of warm EtOH, then adding 25g Na2CO3 dissolved in 400mL of distilled water. The alkaline solution was cooled and extracted six times with 50mL portions of diethyl ether (discarded). Diphenylcarbazone was then precipitated by acidifying the alkaline solution with 3M HNO3 or glacial acetic acid. It was filtered off, air dried, and stored in the dark [Gerlach & Frazier Anal Chem 30 1142 1958]. Other impurities are phenylsemicarbazide and diphenylcarbodiazone. Impurities can be detected by chromatography [Willems et al. Anal Chim Acta 51 544 1970]. It is used for detection and estimation of Hg, Zn, Cd, Cr, Cu, Fe and Mo [Cheng et al. Handbook of Organic Analytical Reagents, Boca Baton 277 1982, Beilstein 16 H 24, 16 IV 17.]
Lastest Price from DIPHENYLCARBAZONE manufacturers
  • Diphenylcarbazone
  • US $15.00-10.00/KG
  • CAS:538-62-5
  • Min. Order: 1KG
  • Purity: 99%+ HPLC
  • Supply Ability: Monthly supply of 1 ton
  • 2021-07-13
  • Diphenylcarbazone
  • US $15.00-10.00/KG
  • CAS:538-62-5
  • Min. Order: 1KG
  • Purity: 99%+ HPLC
  • Supply Ability: Monthly supply of 1 ton
  • 2021-07-09

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  • Company Name:J & K SCIENTIFIC LTD.
  • Tel:010-82848833 400-666-7788
  • Products Intro:Product Name:Diphenylcarbazone, indicator
    CAS:538-62-5
    Purity:60.0%(LC) Package:10G;50G More...
  • CB Index:76
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  • Tel:4006608290; 18621169109
  • Products Intro:Product Name:Diphenylcarbazone
    CAS:538-62-5
    Purity:40% Package:25g;50g Remarks:C53003 More...
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  • Company Name:TCI (Shanghai) Development Co., Ltd.
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  • Products Intro:Product Name:Diphenylcarbazone (contains Diphenylcarbazide)
    CAS:538-62-5
    Purity:40.0% LC Package:25G More...
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  • Company Name:BeiJing Hwrk Chemicals Limted
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  • Products Intro:Product Name:DIPHENYLCARBAZONE
    CAS:538-62-5
    Purity:AR Package:1kg Remarks:HWG08282 More...
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  • Company Name:Energy Chemical
  • Tel:021-021-58432009 400-005-6266
  • Products Intro:Product Name:DIPHENYLCARBAZONE
    CAS:538-62-5
    Purity:60% Package:25G More...
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  • Company Name:Beijing Ouhe Technology Co., Ltd
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  • Products Intro:Product Name:DIPHENYLCARBAZONE
    CAS:538-62-5
    Purity:98% Package:10g;50g;100g;250g;500g More...
  • CB Index:60
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  • Company Name:Shanghai Hanhong Scientific Co.,Ltd.
  • Tel:021-54306202 13764082696;
  • Products Intro:Product Name:Diphenylcarbazone
    CAS:538-62-5
    Purity:40% Remarks:B36156 More...
  • CB Index:64
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