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Methyl acetate

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Methanol in methyl acetate can be detected by measuring its solubility in water. At 20o, the solubility of methyl acetate in water is ca 35g per 100mL, but 1% MeOH confers complete miscibility. Methanol can be removed by conversion to methyl acetate, by refluxing for 6hours with acetic anhydride (85mL/L), followed by fractional distillation. Acidic impurities can be removed by shaking with anhydrous K2CO3 and distilling. An alternative treatment is with acetyl chloride, followed by washing with concentrated NaCl and drying with CaO or MgSO4. (Solid CaCl2 cannot be used because it forms a crystalline addition compound.) Distillation from copper stearate destroys peroxides. Free alcohol or acid can be eliminated from methyl acetate by shaking with strong aqueous Na2CO3 or K2CO3 (three times), then with aqueous 50% CaCl2 (three times), saturated aqueous NaCl (twice), drying with K2CO3 and distilling it from P2O5. [Beilstein 2 IV 122.]
Lastest Price from Methyl acetate manufacturers
  • Methyl acetate
  • US $1.00 /g
  • CAS:79-20-9
  • Min. Order: 1g
  • Purity: 99%
  • Supply Ability: 10 tons
  • 2024-04-23
  • Methyl acetate
  • US $3.90 /kg
  • CAS:79-20-9
  • Min. Order: 1kg
  • Purity: 99.95%
  • Supply Ability: 2000mt/month
  • 2024-02-27

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  • Company Name:Taizhou Mingguang Chemical Co.,Ltd
  • Tel:0523-82569810
  • Products Intro:Product Name:Methyl acetatae
    CAS:79-20-9
  • CB Index:58
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  • Tel: 19102157732
  • Products Intro:Product Name:Methyl acetate
    CAS:79-20-9
    Purity:Standard for GC,≥99.5% Package:5ml Remarks:0.934 g/mLat25°C
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    CAS:79-20-9
    Purity:99.00% Package:180KG
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  • Company Name:Shandong Hexun Energy Technology Co., Ltd
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    Purity:99.9 Package:180KG;1000KG
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  • Company Name:-W&Y Express Chemical Industry Co., Ltd (ShenYang)
  • Tel:024-31124838 15840046119
  • Products Intro:Product Name:Methyl acetate
    CAS:79-20-9
    Purity:99.90% Package:180kg/RMB 5800
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  • Company Name:Wuhan Xinzhongke Chemical Technology Co., Ltd
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    Purity:90% Package:25KG;50KG;100KG
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  • Company Name:Dongying Sifang Litong New Material Co. LTD
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  • Products Intro:Product Name:METHYL ACETATE
    CAS:79-20-9
    Purity:99.5% Package:180kg/桶
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  • Company Name:Shandong Laya Chemical Co., Ltd
  • Tel: 17561421001
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    CAS:79-20-9
    Purity:99.9% Remarks:ton
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