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Glycocholic acid

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USE
Glycocholic acid crystallises from hot water as the sesquihydrate. Dry it at 110o in vacuo. An analytical sample is prepared by suspending the acid (4g) in H2O (400mL) at ~20o, heating to boiling with slow stirring, filtering hot and allowing to cool to ~20o. The acid is filtered off, washed with H2O, dried in air, recrystallised from 5% aqueous EtOH, washed well and dried over P2O5 in a moderate vacuum to constant weight. Recrystallisation from EtOH/EtOAc, and drying, gave the anhydrous acid. [Cortese & Bauman J Am Chem Soc 57 1393 1935, Bergstrom & Norman Acta Chem Scand 7 1126 1953, Beilstein 10 IV 2077.]
Lastest Price from Glycocholic acid manufacturers
  • Glycocholic acid
  • US $0.00-0.00/Kg
  • CAS:475-31-0
  • Min. Order: 1Kg
  • Purity: 99.9%
  • Supply Ability: 200tons
  • 2024-04-08
  • Glycocholic acid
  • US $34.00-1.20/kg
  • CAS:475-31-0
  • Min. Order: 1kg
  • Purity: 99%
  • Supply Ability: g-kg-tons, free sample is available
  • 2024-04-05

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