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METHYLPHOSPHONIC ACID

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Methylphosphonic acid [993-13-5] M 96.0, m 104-106o, 105-107o, 108o, pK 1 2.12, pK 2 7.29. If it tests for Cl-, then add H2O and evaporate to dryness, repeat several times till free from Cl-. The residue solidifies to a wax-like solid. Alternatively, dissolve the acid in the minimum volume of H2O, add charcoal, warm, filter and evaporate to dryness in a vacuum over P2O5. [Kosolapoff J Am Chem Soc 75 3379 1953.] The di-Na salt is prepared from 24g of acid in 50mL of dry EtOH, and a solution of 23g Na dissolved in 400mL EtOH is added. A white precipitate is formed, but the mixture is refluxed for 30minutes to complete the reaction. Filter off the solid and recrystallise it from 50% EtOH. Dry the crystals in a vacuum desiccator. [Thompson J Chem Soc 3292 1952, Beilstein 4 IV 3498.]
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  • Company Name:Shaanxi Xihua Chemical Industry Co., Ltd
  • Tel:029-81123119 15529505138
  • Products Intro:Product Name:Methylphosphonicacid
    CAS:993-13-5
    Purity:98% Package:25KG
  • CB Index:58
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  • Company Name:Tianjin Rongshen Chemical Co., Ltd
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    CAS:993-13-5
    Purity:98% Package:100g
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  • Company Name:J & K SCIENTIFIC LTD.
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  • Products Intro:Product Name:Methanephosphonic acid, 98%
    CAS:993-13-5
    Purity:98% Package:5GR, 25GR More...
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  • Company Name:Meryer (Shanghai) Chemical Technology Co., Ltd.
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  • Products Intro:Product Name:Methanephosphonic acid
    CAS:993-13-5
    Purity:98% Remarks:35433 More...
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  • Company Name:Beijing HwrkChemical Technology Co., Ltd
  • Tel:010-89508211 18501085097
  • Products Intro:Product Name:Methanephosphonic acid
    CAS:993-13-5
    Purity:98.00% Package:5g
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  • Company Name:Energy Chemical
  • Tel:021-021-58432009 400-005-6266
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    Purity:>97% Package:10g,25g,100g,500g,5kg More...
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