2-Bromofluorene
1133-80-8 Basic informationMore
- Product Name:2-Bromofluorene
- Synonyms: 2-Bromofluorene,95% 4-Bromo-2,2'-methylenebiphenyl 2-BroMofluorene, 95% 25GR 2-BroMofluorene, BroMofluorene 2-broMo-2H-fluorene 2-broMo-9H-fluorene (2BF) 2-BroMofluorene, 98.0%(GC) 2-Bromofluorene 95%
- CAS:1133-80-8
- MF:C13H9Br
- MW:245.11
- EINECS:214-480-6
- Mol File:1133-80-8.mol
USE
2-bromofluorene is often used as synthetic intermediate of the OLED material in industry, by the reaction of barbier-type ultrasonic radiation, 2-bromofluorene is also used to study the conversion of aryl bromides to aryl triethoxy silane.<br />
<strong>Lab Preparation Methods:</strong> propylene carbonate is used as solvent, N-bromosuccinimide (NBS) is used as brominated reagent to carry bromination reaction of fluorine, and this reaction can synthesize 2-bromofluorene and 2,7-dibromofluorene. By the investigation of reaction temperature, NBS amount, the adding methods, the optimal reaction conditions for the synthesis of 2-bromofluorene is confirmed. The optimal reaction conditions are: reaction temperature is 23℃, the molar ratio of NBS with fluorine is 1.1:1, NBS is added by stage addition. First fluorene and propylene carbonate is preheated to 60℃, so fluorine is all dissolved, and then it drops to the reaction temperature, NBS is added by stage addition. 2-bromofluorene and 2,7-dibromofluorene recrystallizes with ethanol and acetic acid respectively, the purity of target product of liquid chromatography can reach more than 99%.
Lastest Price from 2-Bromofluorene manufacturers
- 2-Bromofluorene
- US $210.00 /KG
- CAS:1133-80-8
- Min. Order: 1KG
- Purity: 98%
- Supply Ability: 300MT/year
- 2024-12-20
- 2-Bromofluorene
- US $14.00-123.00/g
- CAS:1133-80-8
- Min. Order: 100g
- Purity: 0.98
- Supply Ability: 10kg
- 2024-11-01
Browse by Nationality 1133-80-8 Suppliers >Global suppliers
Beijing (18) Shanghai (102) Tianjin (3) Chongqing (3) Sichuan (6) Guangdong (18) Zhejiang (24) Fujian (7) Hunan (1) Hubei (36) Shandong (12) Henan (28) Hebei (19) Liaoning (4) Heilongjiang (2) Anhui (7) Jiangsu (38) Jiangxi (2) Shaanxi (6) Hong Kong (3) Other (1) Member (323) All (340)
Please select the suppliers
Recommend You Select Member Companies
Recommend You Select Member Companies
- Company Name:Zhengzhou Shengyi New Material Technology Co., LTD
- Tel:0371-63891666 18037898020
- Products Intro:Product Name:2-Bromofluorene
CAS:1133-80-8
Purity:99.9% Package:1kg;25kg - CB Index:58
- Related Information:Catalog(38)
- Company Name:Zhengzhou HQ Material Co., Ltd.
- Tel:0371-67759225 13526468238
- Products Intro:Product Name:2-BroMofluorene
CAS:1133-80-8
Purity:99% Package:1kg;100kg;1T More... - CB Index:55
- Related Information:Catalog(814)
- Company Name:J & K SCIENTIFIC LTD.
- Tel:010-82848833 400-666-7788
- Products Intro:Product Name:2-Bromofluorene, 95%
CAS:1133-80-8
Purity:95% Package:100G;25G;5G More... - CB Index:76
- Related Information:Catalog(96815)
- Company Name:Meryer (Shanghai) Chemical Technology Co., Ltd.
- Tel:021-61259108 18621169109
- Products Intro:Product Name:2-BroMofluorene
CAS:1133-80-8
Purity:97% Package:5g;25g;100g Remarks:AAA123754 More... - CB Index:62
- Related Information:Catalog(40228)
- Company Name:future industrial shanghai co., ltd
- Tel:400-0066400 13621662912
- Products Intro:Product Name:2-Bromofluorene
CAS:1133-80-8
Purity:97% Package:663RMB/ 25g More... - CB Index:65
- Related Information:Catalog(1995)
- Company Name:TCI (Shanghai) Development Co., Ltd.
- Tel:021-67121386
- Products Intro:Product Name:2-Bromofluorene
CAS:1133-80-8
Purity:98.0% GC Package:100G,,25G,5G More... - CB Index:81
- Related Information:Catalog(24529)