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SOLASODINE

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Solasodine crystallises (as monohydrate) from MeOH as lustrous plates (on heating, the plates change to needles as they melt and resolidify in needles), or aqueous 80% EtOH, and sublimes at high vacuum. After recrystallisation from H2O, m 198-199o, then from Me2CO/H2O, m 199-201o, it has [] D 22 -109.3o (c 0.581, CHCl3). On TLC with silica gel G (*C6H6/absolute EtOH, 8:2) it has RF 0.45. IR (KBr): max at 10.3, 10.4, 11.2, 11.5 (azaoxaspirane bands). [Schreiber & Rnsch Tetrahedron 20 1939 1964, Uhle J Org Chem 27 656 1962, Kessar et al. Tetrahedron 27 2153 1971, Beilstein 27 III/IV 2000.]
Lastest Price from SOLASODINE manufacturers
  • SOLASODINE
  • US $0.00-0.00/kg
  • CAS:126-17-0
  • Min. Order: 0.10000000149011612kg
  • Purity: ≥98%HPLC
  • Supply Ability: 20tons
  • 2024-04-26
  • Solasodine
  • US $0.00 /mg
  • CAS:126-17-0
  • Min. Order: 5mg
  • Purity: ≥98%(HPLC)
  • Supply Ability: 10 g
  • 2023-02-24

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