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3,5-Lutidine

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591-22-0 Basic informationMore
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Dry 3,5-lutidine with sodium and fractionally distil it through a Todd column (p 11) packed with glass helices. Dissolve (100mL) in dilute HCl (1:4) and steam distil this until 1L of distillate is collected. Excess conc NaOH is added to the residue which is again steam distilled. The base is extracted from the distillate, using diethyl ether. The extract is dried over K2CO3, and distilled. It is then fractionally crystallised by partial freezing. The hydrochloride has m 229o(sublimes at 190-231o), and the picrate has m 242-243o(dec, from H2O), 249-250o(dec, from AcOH). [Beilstein 20 II 161, 20 III/IV 2788, 20/6 V 60.]
Lastest Price from 3,5-Lutidine manufacturers
  • 3,5-Lutidine
  • US $1.10 /g
  • CAS:591-22-0
  • Min. Order: 1g
  • Purity: 99.00%
  • Supply Ability: 100 Tons min
  • 2021-08-26

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  • Company Name:Changzhou KOYE Chemical Co.,LTD.
  • Tel:519-81882581 18602584369
  • Products Intro:Product Name:3,5-Lutidine
    CAS:591-22-0
    Purity:99% Package:200KG/RMB 1
  • CB Index:58
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  • Company Name:Pand (Shanghai) international trade Co., LTD
  • Tel:18662931292 18662931292
  • Products Intro:Product Name:3,5-Lutidine
    CAS:591-22-0
    Purity:99%含量 Package:1KG;200KG;1000KG
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  • Company Name:Jiangsu Raien Environmental Protection Technology Co., Ltd
  • Tel:0513-0513-66814573 16651336298
  • Products Intro:Product Name:3,5-Lutidine
    CAS:591-22-0
    Purity:99% HPLC Package:1KG;25KG;200KG
  • CB Index:58
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  • Company Name:Jinan Junhe Pharmaceutical Co., Ltd
  • Tel:15653300596 18653300596
  • Products Intro:Product Name:3,5-Lutidine
    CAS:591-22-0
    Purity:99% Package:1KG;10kg;25KG;200kg
  • CB Index:58
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  • Company Name:Meryer (Shanghai) Chemical Technology Co., Ltd.
  • Tel:021-61259108 18621169109
  • Products Intro:Product Name:3,5-Lutidine
    CAS:591-22-0
    Purity:98% Package:25g;100g;500g Remarks:AAA124638 More...
  • CB Index:62
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  • Company Name:TCI (Shanghai) Development Co., Ltd.
  • Tel:021-67121386
  • Products Intro:Product Name:3,5-Lutidine
    CAS:591-22-0
    Purity:98.0% GC Package:25ML,500ML More...
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