Julolidine
479-59-4 Basic informationMore
- Product Name:Julolidine
- Synonyms: JULOLIDINE 2,3,6,7-TETRAHYDRO-1H,5H-BENZO[IJ]QUINOLIZINE 2,3,6,7-TETRAHYDRO-1H,5H-PYRIDO[3.2.1-IJ]QUINOLINE 1H,5H-BENZO[IJ]QUINOLIZINE, 2,3,6,7-TETRAHYDRO- 5h-benzo[ij]quinolizine,2,3,6,7-tetrahydro-1 Julolidine,98% 2,3,6,7-Tetrahydro-1H,5H-benzop[ij]quinolizine Julolidine, 98% 25GR
- CAS:479-59-4
- MF:C12H15N
- MW:173.25
- EINECS:207-535-0
- Mol File:479-59-4.mol
-
USE
Purify julolidine by dissolving it in dilute HCl, steam is bubbled through the solution and the residual acidic solution is basified with 10N NaOH, extracted with Et2O, washed with H2O, dried (NaOH pellets), filtered, evaporated and distilled in vacuo. The distillate crystallises on cooling (m 39-40o). It develops a red colour on standing in contact with air for several days. The colour can be removed by distilling or dissolving in 2-3 parts of hexane, adding charcoal, filtering and cooling in an Me2CO/Dry-ice bath when julolidine crystallises out (85-90% yield m 39-40o). The hydrobromide [83646-41-7] has m 218o (239-242o), the picrate has m 174o(165o) and the methiodide crystallises from MeOH, with m 186o [Glass & Weisberger Org Synth Coll Vol III 504 1955, Smith & Yu J Org Chem 17 1285 1952, Beilstein 20 H 332, 20 I 133, 20 II 214, 20 III/IV 3281.] Highly TOXIC.
Lastest Price from Julolidine manufacturers
- Julolidine
-
- US $1.00 /KG
- CAS:479-59-4
- Min. Order: 1g
- Purity: 99.0%
- Supply Ability: 100kg
- 2020-01-13
Browse by Nationality 479-59-4 Suppliers >Global suppliers
Beijing (7) Shanghai (32) Tianjin (4) Guangdong (3) Zhejiang (3) Fujian (3) Hubei (3) Shandong (4) Henan (6) Hebei (1) Anhui (3) Jiangsu (12) Shaanxi (2) Member (82) All (83)
Please select the suppliers
Recommend You Select Member Companies
Recommend You Select Member Companies
- Company Name:Tianjin Nuokang Pharmaceutical Technology Co., Ltd.
- Tel:022-23989838 13810451150
- Products Intro:Product Name:julolidine
CAS:479-59-4
Purity:99% HPLC Package:25g;100g;1000g;25kg - CB Index:58
- Related Information:Catalog(1909)
- Company Name:Yantai Shengkailun Chemical Technology Co., Ltd.
- Tel: 15552437730
- Products Intro:CAS:479-59-4
Package:1g/RMB 1 - CB Index:58
- Related Information:Catalog(9167)
- Company Name:J & K SCIENTIFIC LTD.
- Tel:010-82848833 400-666-7788
- Products Intro:Product Name:Julolidine, 98%
CAS:479-59-4
Purity:98% Package:25G;5G More... - CB Index:76
- Related Information:Catalog(96815)
- Company Name:Meryer (Shanghai) Chemical Technology Co., Ltd.
- Tel:021-61259108 18621169109
- Products Intro:Product Name:Julolidine
CAS:479-59-4
Purity:>97.0%(GC)(T) Package:5g;25g Remarks:J0007 More... - CB Index:62
- Related Information:Catalog(40228)
- Company Name:TCI (Shanghai) Development Co., Ltd.
- Tel:021-67121386
- Products Intro:Product Name:Julolidine
CAS:479-59-4
Purity:97.0% GC&T Package:25G,5G More... - CB Index:81
- Related Information:Catalog(24529)
- Company Name:Beijing HwrkChemical Technology Co., Ltd
- Tel:010-89508211 18501085097
- Products Intro:Product Name:Julolidine
CAS:479-59-4
Purity:NA - CB Index:55
- Related Information:Catalog(8418)