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KAINIC ACID

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Purify the acid by adsorbing on to a strongly acidic ion-exchange resin (Merck), elute the diacid with aqueous M NaOH, the eluate is evaporated, H2O is added, and filtered through a weakly acidic ion-exchange resin (Merck). The filtrate is then evaporated and recrystallised from EtOH. Its solubility is 0.1g in 1mL of 0.5N HCl. (±)--Kainic acid is recrystallised from H2O with m 230-260o. UV (MeOH): 219 (log 3.9); max 1HNMR (CCl4, 100MHz, Me4Si standard) : 1.64 (s 1H), 1.70 (s 3H), 3.24 (d J 7.5, 2H), 3.3-4.2 (1H), 3.70 (s 3H), 3.83 (s 3H), 4.35 (dd J 7.5, J 14.5, 1H), 5.21 (t J 7.5, 1H), 7.26 (t J 7.5, 1H). [Oppolzer & Andres Helv Chim Acta 62 2282 1979, Beilstein 22 III/IV 1523.]

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  • Company Name:Guangzhou Younan Technology Co., Ltd
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  • Products Intro:Product Name:Kainic acid
    CAS:487-79-6
    Purity:98% Package:5mg;10mg;50mg;100mg
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    CAS:487-79-6
    Purity:>99% Package:100Mg,200Mg,25Mg More...
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    Purity:99% HPLC Package:1Mg ; 5Mg;10Mg ;100Mg;250Mg ;500Mg ;1g;2.5g ;5g ;10g More...
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  • Company Name:Finetech Industry Limited
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  • Products Intro:Product Name:KAINIC ACID
    CAS:487-79-6
    Purity:98% Package:1g,10g,25g,500g,1kg
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  • Company Name:Shanghai Macklin Biochemical Co.,Ltd.
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  • Products Intro:Product Name:Kainic Acid
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    Purity:95% Package:1g/ More...
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