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Phenylhydrazine hydrochloride

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Dissolve 100g of phenylhydrazine hydrochloride in 200mL of warm H2O (60-70o) during 1-3hours, then add 1L of boiling EtOH. The solution is filtered, while still hot, through Whatman No 2 filter paper and cooled in a refrigerator. The precipitate is collected on a medium sintered-glass filter and recrystallised twice this way, then washed with cold EtOH, dried thoroughly and stored in a stoppered brown bottle. [Peterson et al. Anal Chem 29 144 1957.] Hough, Powell and Woods [J Chem Soc 4799 1956] boiled the hydrochloride with three times its weight of water, filtered hot (charcoal), added one-third volume of concentrated HCl and cooled to 0o. The crystals were washed with acetone, and dried over P2O5 under vacuum. The salt has also been crystallised from 95% EtOH, and it can be sublimed. [Coleman Org Synth Coll Vol I 442 1941, Beilstein 15 III 71.]
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  • Company Name:3B Pharmachem (Wuhan) International Co.,Ltd.
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  • Products Intro:Product Name:Phenylhydrazine hydrochloride
    CAS:59-88-1
    Purity:99% HPLC Package:1Mg ; 5Mg;10Mg ;100Mg;250Mg ;500Mg ;1g;2.5g ;5g ;10g More...
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  • Products Intro:Product Name:Phenylhydrazine hydrochloride
    CAS:59-88-1
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  • Company Name:WUHAN JIXINYIBANG BIOTECHNOLOGY .,LTD
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  • Products Intro:Product Name:Phenylhydrazine hydrochloride
    CAS:59-88-1
    Purity:99% HPLC Package:1kg;200kg;1000kg
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  • Products Intro:Product Name:PhenylhydraziniuM Chloride
    CAS:59-88-1
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  • Products Intro:Product Name:Phenylhydrazine hydrochloride
    CAS:59-88-1
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  • Products Intro:Product Name:Phenylhydrazine Hydrochloride
    CAS:59-88-1
    Purity:98.5% T Package:100G,25G More...
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