BATHOPHENANTHROLINEDISULFONIC ACID DISODIUM SALT TRIHYDRATE

BATHOPHENANTHROLINEDISULFONIC ACID DISODIUM SALT TRIHYDRATE 화학적 특성, 용도, 생산

• 화학적 성질

  slightly pinkish-beige powder

• 용도

  Bathophenanthrolinedisulfonic acid disodium salt trihydrate was used in double electrochemical covalent coupling method for the fabrication of sensitive amperometric immunosensor, which was based on electro-click chemistry and diazonium chemistry. It was also used in an experimental study based upon, correlating the iron content with the activity, preparation and reconstituting the apoenzyme phenylamine hydroxylase.

• 정의

  ChEBI: An organic sodium salt having 4,7-diphenyl-1,10-phenanthroline 4',4''-disulfonate as the counterion.

• 일반 설명

  Bathophenanthrolinedisulfonic acid disodium salt forms water soluble complexes with palladium and their catalytic role in oxidation of 2-hexanol has been examined.

• Purification Methods

  Dissolve crude sample in the minimum volume of water and add EtOH to precipitate the contaminants. Carefully evaporate the filtrate to obtain pure material. It forms a dark red complex with Fe2+ with 535nm ( 2.23 x 104mol-cm -1) [Imasaka et al. Anal Chim Acta 115 407 1980]. It is prepared by sulfonating bathophenanthroline with ClSO3H: to 100g of bathophenanthroline is added 0.5mL of Fe free ClSO3H and heated over a flame for 30seconds. Cool and carefully add 10mL of pure distilled H2O and warm on a water bath with stirring till all solid dissolves. A stock solution is made by diluting 3mL of this reagent to 100mL with 45% aqueous NaOAc, filter off the solid and store in a dark bottle. In this way it is stable for several months. [Landers & Bennie Am J Clinical Pathology 29 590 1958.]

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