N-シクロヘキシル-N'-(2-モルホリノエチル)カルボジイミド

N-シクロヘキシル-N'-(2-モルホリノエチル)カルボジイミド 価格

N-シクロヘキシル-N'-(2-モルホリノエチル)カルボジイミド 化学特性,用途語,生産方法

• 定義

  ChEBI: A carbodiimide having cyclcohexyl and 2-(4-morpholinyl)ethyl as the two N-substituents.

• Synthesis Reference(s)

  Synthesis, p. 520, 1987 DOI: 10.1055/s-1987-27992

• 合成

  The Preparative Methods of 1-cyclohexyl-3-(2-(4-morpholinyl)ethyl)carbodiimide: from cyclohexyl isothiocyanate and N-(2-aminoethyl)morpholine (67% yield) by dehydration of the corresponding urea with p-Toluenesulfonyl Chloride, Potassium Carbonate, and Benzyltriethylammonium Chloride (91% yield); or by the reaction of cyclohexyl isocyanate, 2-(4-morpholinyl)ethyl diethylphosphoramidate, and potassium carbonate (82% yield).

• 参考文献

  1. For general reviews on the use of carbodiimides, see (a) Kurzer, F.; Douraghi-Zadeh, K. CRV 1967, 67, 107. (b) Williams, A.; Ibrahim, I. T. CRV 1981, 81, 589. (c) Mikolajczyk, M.; Kielbasinski, P. T 1981, 37, 233.
  2. Sheehan, J. C.; Hlavka, J. J. JOC 1956, 21, 439.
  3. Jászay, Z. M.; Petneházy, I.; T?ke, L.; Szajáni, B. S 1987, 520.
  4. Jászay, Z. M.; Petneházy, I.; T?ke, L.; Szajáni, B. S 1988, 397.

N-シクロヘキシル-N'-(2-モルホリノエチル)カルボジイミド 上流と下流の製品情報

N-シクロヘキシル-N'-(2-モルホリノエチル)カルボジイミド 生産企業

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