2-AMino-5-chloro-4'-hydroxybenzophenone

2-AMino-5-chloro-4'-hydroxybenzophenone 化学特性,用途語,生産方法

• 製造方法

  Preparation by cleavage of 5-chloro-3-(phydroxyphenyl)- 2,1-benzisoxazole (other name: 5-chloro-3-(p-hydroxy-phenyl)anthranil) (SM),
  ? by heating at reflux with aluminium iodide for 50 min (87%);
  ? by reaction with concentrated hydrochloric acid and an excess of tin in boiling ethanol or acetic acid. SM (m.p. 241°) was prepared by condensation of o-nitrobenzaldehyde with phenol in the presence of hydrogen chloride or phosphorous oxychloride in cold acetic acid;
  ? by hydrogenation in the presence of 10% Pd/C in ethyl acetate between 40° and 60° at a pressure of 3 atmospheres (quantitative yield).

2-AMino-5-chloro-4'-hydroxybenzophenone 上流と下流の製品情報

2-AMino-5-chloro-4'-hydroxybenzophenone 生産企業

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