Preparation
(1) 4-(2,4-Dinitrophenylamino)phenol and Sodium hydroxide and water is heated to 105 ℃, then add glucose, Sodium sulfide, sulphur and a small amount of Copper sulfate monohydrate, short time boiling, in 20 hours heating to 260 ~ 270 ℃ and roasting 6 hours; (2) (1) the improvement and Sodium hydroxide solution after boiling, with acid precipitation generated degradation products and filtering, will the paste which add to the above Sodium polysulfide solution. Molten material of save glucose also can get similar dye. Further change the above operation process is to use ?4-(2,4-Dinitrophenylamino)phenol?(by 2-Aminophenol and 1-Chloro-2,4-dinitrobenzene obtained) instead of 4-(2,4-Dinitrophenylamino)phenol.
