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氯磷酸二乙酯

产品名称 氯磷酸二乙酯

CAS号814-49-3

分子式C4H10ClO3P

分子量172.55

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  • Mass

    MS-KW-0098          
    diethyl chlorophosphate
    C4H10ClO3P          (Mass of molecular ion:    172)
    

       Source Temperature: 240 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       2.9
          26.0       4.0
          27.0      17.1
          28.0      12.0
          29.0      29.5
          30.0       1.3
          31.0      16.6
          36.0       1.8
          42.0       1.0
          43.0       6.8
          44.0       2.7
          45.0      31.5
          47.0       5.4
          63.0       2.2
          64.0       3.8
          65.0       8.6
          66.0       1.2
          81.0      21.9
          83.0       1.2
          91.0       7.4
          93.0       1.3
          99.0      13.9
         100.0      28.4
         101.0       9.1
         102.0       9.4
         103.0       1.6
         109.0      15.9
         117.0     100.0
         119.0      33.2
         127.0       6.9
         128.0      10.2
         129.0      31.4
         130.0       3.7
         131.0      10.7
         135.0       1.0
         137.0       2.9
         143.0       9.3
         144.0       2.2
         145.0      66.9
         146.0       2.3
         147.0      21.2
         157.0       1.9
         161.0       1.6
         173.0       2.2
         179.0       2.1
         180.0       1.2
         197.0       1.9
         225.0       1.1
         253.0       1.1
         263.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C4 H10 Cl O3 P 0.05 ml : 0.5 ml CDCl3
    diethyl chlorophosphate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.282 B 1.419

         Hz     ppm     Int.
    

       1732.30   4.335     69
       1729.37   4.328    106
       1725.22   4.317     87
       1723.51   4.313    134
       1722.29   4.310    274
       1719.97   4.304    118
       1718.14   4.300     68
       1716.43   4.295    284
       1715.21   4.292    290
       1714.23   4.290    163
       1712.89   4.286    270
       1711.30   4.282     62
       1710.82   4.281     61
       1709.35   4.278    268
       1708.01   4.274    156
       1707.15   4.272    281
       1705.69   4.268    280
       1704.22   4.265     73
       1702.39   4.260    114
       1700.07   4.254    259
       1698.73   4.251    129
       1697.02   4.247     86
       1692.99   4.237     97
       1689.94   4.229     69
        574.95   1.439    633
        573.73   1.436    605
        571.29   1.430     98
        567.87   1.421   1000
        566.65   1.418    968
        562.50   1.408    100
        560.79   1.404    581
        559.57   1.401    593
    

in CDCl3



liquid film





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